GCMS analysis results for sample AE00106, Feb 2002

NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02JAN25\00106.D Vial: 5 Acq On : 25 Jan 2002 1:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 6 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

5.89 3.34 ug/L 1489130 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ . .. 174 C8H14O4 015745-87-6 33 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 32 4 Silane, tetramethyl- (CAS) $$ Te... 88 C4H12Si 000075-76-3 9 Abundance Scan 220 (5.885 min): 00106.D (-) m/z 73.10 100.00% 73

5000

n/z-> 43

armor.. 11011.155. —P . 87 103 I 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 ■ I i ■ ■ ■ ■ i ■ ■ ■ ■ r ' ■ ■ r ■ ■' r ■ ■ ■ i • • • ■ i m/z 5.60 43.10 L 5.80 6 00 6.20 25.36% Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 • ■ • ■ | ‘ 1~ ■ • • ■ । . | . r l . 5.60 5.80 6.00 6.20 43 m/z 45.10 9.59%

n/z-> 27 ।i ■ ■ ■ • । 55 THpn +7 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 113 r"'i ।■ i■ ’ ’■ i ■ ■ ■ ■ । 174 i" •11 •

Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1 -p... 78

5.60 5.80 6.00 6.20 5000 m/z 41.10 9.36% 43

m/z-> 27 55 . . ....... +4+87 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 113 i1 ■■11 r " ■ i" " r " ■ i 174 i■■■ ■ i ■

Abundance #4814: Silane, tetramethyl- 73 5.60 5.80 6.00 6.20 m/z 71.10 6.54%

5000

45 15 ri ■ " ■ i | 53 1 Pi 11 1 88 11 ■ 111 1" r " ■ I " ■' r " ' r " ' i" ■ ■ i' " ■ I" 1 r"■i■■"r"■i■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

00106.D SCAN508.M Mon Jan 28 09:49:53 2002 Page 8

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