GCMS analysis results for sample AE00106, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN25\00106.D Vial: 5 . Acq On : 25 Jan 2002 1:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 4-(Dimethylamino)-1,3-diaza... Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

9.55 0.07 ug/L 32446 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4-(Dimethylamino)-1,3-diazaspiro... 209 C11H19N3O 000000-00-0 74 2 2-Propanol, l,l'-oxybis- (CAS) $... 134 C6H1403 000110-98-5 9 3 PROPENE 3,3,3-D3 45 C3H3D3 001517-51-7 7 4 (1-D)ethenol $$ Ethen-l-d-ol (CAS) 45 C2H3DO 090134-16-0 5 Abundance Scan 541 (9.550 min): 00106. D (-) m/z 59.10 100-00% 59 45

5000

, 1 73 103

9.20 m/z 9.40 45.10 _M 9.60 9.80 68.95% ‘ I‘

n/2-> 20 40 60 80 100 120 140 160 180 200 Abundance #128682:4-(Dimethylamino)-1,3-diazaspiro[4,6]undec-3-en-2-on 59

45 5000 __ __ ____ A, 9 20 9.40 9.60 9.80 73 m/z 103.10 48.89% । 103 | | 209 0 >!■■■• | ' । . I ( 'i । । । । । m/z--> 20 40 60 80 100 120 140 160 180 200 Abundance #29204: 2-Propanol, 1,1'-oxybis- (CAS) $$ Dipropylene glyc... 59 .......... fl.... 9.20 9.40 9.60 9.80 31 m/z 73.10 48.50% 5000 45 103

i, ....... ■ ■ ■ i ■ ■ ' ■ i n/z-> Abundance 20 40 60 80 100 120 140 #174: PROPENE 3.3.3-D3 160 180 200 NNA ' I ' ' ' ' I ' ' ' 9.20 9.40 9.60 9.80 m/z 41.10 30.29%

m/z--> 5000

27 ,11161 . .il ,. 20 40 60 80 100 120 140 160 180 200 TTI 9.20 9.40 4 9.60 9.80 IT

30106.D SCAN508.M Mon Jan 28 09:49:53 2002 Page 9

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