GCMS results for sample AE00463, Jan 24 2002

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Laboratory report showing GCMS analysis of sample AE00463 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051422–000051438

Folder label: “GCMS X 1/8/02 A 1/11/02”

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NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\5973N\02JAN11\00463.D Vial: 5 Acq On : 11 Jan 2002 5:25 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak. Number 6 4 - (Dimethylamino)-1,3-diaza .. . Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 9.64 0.10 ug/L 31452 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-(Dimethylamino)-1,3-diazaspiro. . . 209 C11H19N3O 000000-00-0 78 2 Ethane, 1-ethoxy-l-methoxy- 104 C5H12O2 010471-14-4 9 3 E-Dipropylene glycol $$ 2-hydrox... 134 C6H14O3 000000-00-0 9 4 2-Propanol, l,l'-oxybis- (CAS) $... 134 C6H1403 000110-98-5 9 Abundance Scan 549 (9.642 min): 00463.D (-) m/z 59.10 100.00% 53

M. 103 5000 73 1 ' i 1 ri 1 r1■ ' • i • ' 9.40 9.60 9.80 10.00 o 84 m/z 45.10 53.91% I'1' ‘ I 'i""i"r"■ i""r "■ i"‘■ I"■11"'■ t 111 ‘' I" 111 H '11 m/z-> :20 30 40 50 60 70 80 90 100110120130140150160170180190200 210 Abundances #128682: 4-(Dimethylamino)-1,3-diazaspiro[4,6]undec-3-en-2-on 50 45 - 5000 9.40 9.60 9.80 10.00 73 m/z 103.10 50.46% 103 O-mm |"‘‘..... ............ I...................................... 1‘"1‘0111‘0111110U00TOTI0TTE01EI0 209 TTT >| > ! Ti ‘E"O"T‘‘"ETTO—OI"CA"IT"TOT"I‘"F m/z-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200 210 Abundance #10235: Ethane, 1 -ethoxy-1 -methoxy- 59 45 9.40 9.60 9.80 10.00 5000 m/z 73.10 35.69% 73 89 27

n/z-> o :20 LL 103 Tuur " " I ■ ' I'' " 11"' I" " I " " I" " I" " I" " I" " I" " I" " I " " I'1'11" " I ’ ‘" I 30 40 50 60 70 80 90 100110120130140150160170180 190 200 210 Abundance ............ ..................... ..... , #29239: E-Dipropylene glycol $$ 2-hydroxyethyl ether 31 59 9.40 9.60 9.80 10.00 m/z 41.10. 30.62% 5000 45 A 103

0 ■ ।" i ■ i +rTmmmmmmmmmmmmmm TTI " I" ′′ l-Cl T‘ I "TI I ! 'I /z-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 9.40 9.60 9.80 10.00

00463.D SCAN508.M Mon Jan 14 10:46:57 2002 Page 8

NYC-WTC_000051433

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