GCMS results for sample AE00463, Jan 24 2002

NYC 9/11 Public Portal Document

Llprary Searcn Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN11\00463.D Vial: 5 Acq On : 11 Jan 2002 5:25 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L Peak Number 5 2-Butanol, 3,3'-oxybis- Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 9.55 0.11 ug/L 33505 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Butanol, 3,3'-oxybis- 162 C8H18O3 054305-61-2 9 2 E-Dipropylene glycol $$ 2-hydrox... 134 C6H14O3 000000-00-0 9 3 BIS(1-METHYL-2 -HYDROXYETHYL)ETHER 134 C6H14O3 000000-00-0 9 4 2-Propanol, l,l'-oxybis- (CAS) $... 134 C6H14O3 000110-98-5 9 Abundance Scan 541 (9.550 min): 00463.D (-) m/ z 59.10 100.00% 59 ■ • _

5000 45 103 73

84 9.20 9.40 9.60 9.80 Oh-........ 1 ■ । 1 ■ ■ 1 i 1 1 1 1 i 1 1 1 ' i 11 1 ■ i ■ 1 ■ 1 । ■ ■ ■ ■ i 1 1 1 1 । ■ ■ ■ ■ । ' m/z 103.10 41.93% m/z-> 20 30 60 70 80 90 100 110 120 130 140 Abundance #61826: 2-Butanol, 3,3'-oxybis- 59

5000 31 45 103 9.20 9.40 9.60 9.80 m/z 45.10 40.35%

mlz-> 0— 20 30 —40+ r.50 —(60T 70 134 » i ■ • ■ • i ■ • ■ 11 ■ ■ ■ ■ i > 1 ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i • ■ ■ ■ i • 80 90 100 110 120 130 140 Abundance #29239: E-Dipropylene glycol $$ 2-hydroxyethyl ether 31 59 T IT 9.20 9.40 9.60 9.80 5000 m/z 73.10 27.49% 45 103 39,

n/z~> 0 ---PH III..... ................................ 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #29208: BIS(1-METHYL-2-HYDROXYETHYL)ETHER I 1 1 1 1 1 1 ' ■ 1 r1 1 • 1 1 1 59 9.20 9.40 9.60 9.80 m/ z 41.00 23.91% 5000 31 45 103

134 0 --- ■ 1 । 11 ■''1 ■ ।। । > ■' > । ■' ■ ■ । > 1 ■ ■ i 11 ■ > i 1 1 1 1 i ■ 1 ■ 1 i ■ m/z-> 20 30 40 50 (60 70 80 90 100 110 120 130 140 9.20 9.40 9.60 9.80

00463.D SCAN508.M Mon Jan 14 10:46:57 2002 Page 7

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