GCMS analysis results for sample AE00308, Jan 2002

NYC 9/11 Public Portal Document

Llbrary searcn Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN08\308.D Vial: 7 Acq On 8 Jan 2002 10:28 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 Butenol, methyl- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 4.99 0.14 ug/L 46061 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butenol, methyl- 86 C5H10O 060766-00-9 2 3-hydroxy-4,4-dimethyl .gamma. B. . . 130 C6H10O3 052126-90-6 3 Butane, 2,2-dimethyl- 86 C6H14 000075-83-2 9 4 DEUTEROACETONE 59 C3H5DO 004468-52-4 7 Abundance Scan 142 (4.995 min): 308. D (-) m/z 43.10 100.00% 43 71

5000 39 59 A/A) , -A 55 4.60 4.80 5.00 5.20 5.40 84 m/z-> 5 1. . ob ■' i " " i " '' r " ' r " ‘ i " " i " ‘ I’’ 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 ■111 ■ ■ ■ । ■u 1111 ■ ■ ।11 ■' । m/ z 71.10 98.50% Abundance #4093: Butenol, methyl-

5000

15 27 31 671 43

86 53 59 71

A 4.60 4.80 5.00 m/z 41.10 5.20 5.40 53.41%

m/z-> Or ’ I’’ " i ■ " ■ r... i. TII|.4 -Hr " I'.' ■ i T+ 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 IT

Abundance #26149: 3-hydroxy-4,4-dimethyl .gamma. Butanolactone $$ Pa... 43 7h q 4.60 4.80 5.00 5.20 5.40 5000 m/z 69.10 45.00% 57 31 53 68 mm — — m/z- > 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #4273: Butane, 2,2-dimethyl- 1’’ । > < > ■ । > > 43 57 71 4.60 4.80 5.00 5.20 5.40 m/ z 59.00 34.96% 5000 29

53 ----------------------- op " i " " i ‘ ' i" " i' TT’’ 1111111 ...... HP +TTTTTTTTTTTT m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 4.60 4.80 5.00 5.20 5.40

508.D SCAN508.M Wed Jan 09 15:17:07 2002 Page 6

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