GCMS analysis results for sample AE00308, Jan 2002

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Laboratory report showing GCMS analysis of sample AE00308 for unknown compounds and DDD on January 10, 2002.

NYC-WTC_000051073–000051087

Folder label: “GCMS X 1/7/02 A 1/8/02”

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NYC 9/11 Public Portal Document

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Data File : C : \MSDCHEM\1\5973N\02JAN08\308 . D Vial: 7 Acq On : 8 Jan 2002 10:28 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 5 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 5.89 4.51 ug/L 1478340 1,4-Dichlorobenzene-d4 9.71 ( Hit# of 5 'entative ID MW MolForm CAS# Qual 1Acetic acid, 3- [1,3] dioxolan-2-y. . . 174 C8H14O4 000000-00-0 2.3-(CYCLOHEX-3 ‘-EN-YL) PROPANOL $$... 174 C8H1404 015745-87-6 3 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 33 4 Silane, tetramethyl- Abundance 3— —A $$ Tetramet... Scan 220 (5.885 min): 308.D (-) 88 C4H12Si 000075-76-3 25 m/z 73.10 100.00% 73

5000 43 55 87 103 5.60 5.80 6.00 6.20 n/z-> 0- PP.. I, r M*** ' - TT PT TTTT i' ■ ■ ■ i I ' '' ' I'' '' I m/z 43.10 24.65% 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 110 I , । । . । 1r. . . 5.60 5.80 6.00 6.20 43 m/z 41.10 9.38% 27 55 87 113 174 0-TTT ' i ■ ■ ■11'1'' i' +TT '1' i'' ■ ' i ■ ■ • ■ i ■ • ■' i ■1'11'11' I I" 1' I 111' n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 -----PPp* 5.60 5.80 6.00 6.20 5000 m/z 45.10 8.96% 43 27 87 113 011 1 1 1 ''' I 1 TT14 11 "55■ ■ i " 1 'i' TTT P1mpuuuuUmOnTDTT 174 I‘|1 n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #9702: Butane, 2-methoxy-2-methyl- $$ Ether, methyl tert-p... 7(3 5.60 5.80 6.00 6.20 m/z 71.10 6.10%

5000 55 87

m/z-> 27 45 0 1 r 1 ■'I 11 * " p. ‘ I ■11" 20 30 40 50 60 m 70 । " i' " 111" 111 " 1111 " 11 rri r " 11'11111'1 ■ 111 ■ ■ i'r 111' 80 90 100 110 120 130 140 150 160 170 180 ----- 5.60 5.80 6.00 6.20

308.D SCAN508.M Wed Jan 09 15:17:08 2002 Page 7

NYC-WTC_000051083

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GCMS analysis results for sample AE00309, Jan 2002 · Box DEP Box 28

NYC-WTC_000051088

Laboratory report showing GCMS analysis of sample AE00309 for unknown compounds and DDD on January 10, 2002.

1 shared topics · Same agency, volume and box · similarity 0.997