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GCMS analysis results for sample AE03245, March 2002

Machine-extracted title · confidence 95%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03245 conducted on March 15, 2002.

NYC-WTC_000006085–000006104

Folder label: “GCMS X 2/12/02 A 3/01/02

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Scanned page image, NYC-WTC_000006100
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02MAR01\03245.D Vial: 6 ' Acq On : 1 Mar 2002 2:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.89 4.84 ug/L 2146070 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H1404 000000-00-0 33 23-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 3 Silane, tetramethyl- $$ Tetramet... 88 C4H12Si 000075-76-3 28 4 Silane, tetramethyl- (CAS) $$ Te... 88 C4H12Si 000075-76-3 9 Abundance Scan 223 (5.891 min): 03245.D (-) m/ z 73.10 100.00% 7)3

5000 43 5.60 5.80 6.00 6.20 O-T 1,1 55.65 1’11 1 11" ‘ I ’11 11 1 87 103 111111a1|dum m/z 43.10 23.51% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1 ,3]dioxolan-2-ylpropyl ester 73

5000 5.60 5.80 6.00 6.20 43 m/z 45.10 9.52% 27 87 0- TTr 55 , । . ........ 113 IIIIIIII’IIIIIIIII 174 miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 7f3 HI’t 5.60 5.80 6.00 6.20 5000 m/ z '41.10 ■ 9.05%

43 27 87 01 mpm 11"55" i " ' 111Pmmm113 , i 174 I‘ ‘ISIAAAA**3/AA*/// n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4812: Silane, tetramethyl- $$ Tetramethylsilane $$ (CH3)4... 11 I 1 ' ' ' T 1 1 IM Pr 1 vr 73 5.60 5.80 6.00 6.20 m/z 71.00 6.67%

5000

45 15 31 | 55 1 88 0 111" I " i1 " ' i' TTTTTTTm —’——0—000000—— 1 r i 1 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

3245.D HP022102.M Mon Mar 04 12:33:06 2002 Page 12

NYC-WTC_000006100

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NYC-WTC_000006100Source: NYC Law Department, mirrored locally

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