GCMS analysis results for sample AE03245, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03245 conducted on March 15, 2002.

NYC-WTC_000006085–000006104

Folder label: “GCMS X 2/12/02 A 3/01/02”

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NYC 9/11 Public Portal Document tpOuiIU RCDOL L

Data File : C: \MSDCHEM\1\5973N\02MAR01\03245.D Vial: 6 Acq On : 1 Mar 2002 2:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 3-Penten-2-ol (CAS) $$ 2-PE... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 5.72 0.06 ug/L 25258 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Penten-2-ol (CAS) $$ 2-PENTEN-... 86 C5H10O 001569-50-2 56 2 Trifluoroacetic acid, 2-tetrahyd... 198 C7H9F3O3 000000-00-0 9 3 4-Penten-2-ol (CAS) $$ PENT-4-EN... 86 C5H10O 000625-31-0 7 4 3-Buten-2-ol, 2-methyl- (CAS) $$... 86 C5H10O 000115-18-4 7 Abundance Scan 208 (5.722 min): 03245.D (-) m/z 41.10 100.00% 41 71

5000

"1 । ■ ■ ' 1 11 1 1 11T r 1 । 49 86 5.40 5.60 5.80 6.00 0 ' ' T’’ i > | i ‘ | ‘ H i | > l> ' ]1 1i i| l >i | TH ' i' •" r "11" ‘ mhmmmmmmmm m/ z 71.10 84.12% /z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #4043: 3-Penten-2-ol (CAS) $$ 2-PENTEN-4-OL $$ Methyl prop... 43 71

5000 27 T-r-f-r-r "’ I 5.40 5.60 5.80 6.00 15 53 m/ z 43.05 73.83% 58 86

n/z-> Of "r i ■1" —R 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 11" i' ।11 > j < 11 ■ 111 <. ।. 1111 -mmmp

Abundance #111395: Trifluoroacetic acid, 2-tetrahydrofurylmethyl ester 43 71 IITIPT’E IITTT 5.40 5.60 5.80 6.00 5000 m/z 69.10 35.78% 31 51 .............................. 37 ] 1 1 I I I] I I 1 I | 57 1 I I > | I |-TT| I I I I | , 95 0-TTTTETTTTWTTTTTTTTTTT TTTITTT m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #4058:4-Penten-2-ol (CAS) $$ PENT-4-EN-2-OL $$ 1-Penten-4... 43 71 5.40 5,60 5.80 6.00 m/ z 45.10 27.80%

5000

27 I 53 58 86 Of" " i " " i1 ■" i" " i'11 " i" " r 371'' i ,1 - 1111111' m 11111111111,1111111111

mfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 5.40 5.60

>3245.D HP022102.M Mon Mar 04 12:33:06 2002 Page 11

NYC-WTC_000006099

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