GCMS results for sample AE00739, Jan 29 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN16\00739.D Vial: 7 . Acq On : 16 Jan 2002 8 : 07 pm Operator: Sample : 508scan Inst : Instrumen Mise 2002 : January 16, Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 3-Penten-2-ol Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

4.62 0.12 ug/L 42724 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Penten-2-ol 86 C5H10O 001569-50-2 49 2 3-PENTEN-2-OL, (Z) - 86 C5H10O 024652-50-4 49 3 2-Buten-l-ol, 3-methyl- 86 C5H10O 000556-82-1 43 42-Buten-1-ol,3-methyl-(CAS)$$...86C5H100 Abundance Scan 109 (4,618 min): 00739.D (-) m/z 000556-82-1 43 71.10 100.00% 57 71 41 88 5000

44 53 68 85 A.,, I m/z-> Ol 111' ■ ’' i ■ ■ ■11' ■ ■' i ■ ■ 20 25 30 35 40 + 45 50 55 ■ । ■ ■ > ■ ।1 1'11 60 65 70 75 80 11 111'11 ' I 85 ■ i' ' ■ ■ i' ■ 90 95 4.20 m/z 4.40 57.10 4.60 4.80 5.00 86.48% Abundance #4046: 3-Penten-2-ol 7h 43

5000 39 _A 53 67 4.20 4.40 4.60 4.80 5.00 27 m/z 41.10 79.23% Ol ■' i1'' ' i ' ' ' T । 1 1 1 | 1 1 1 T‘ 58 .LT. Hi. I 86 1 m/z-> 75 80 85 90 95

AAAM 20 25 30 35 40 45 50 55 60 65 70 Abundance #4208: 3-PENTEN-2-OL, (Z)- 7h 43 4.20 4.40 4.60 4.80 5.00 5000 39 m/z 88.00 61.39% 53 67 27

m/z-> 20 ol TTTPTTTT 25 30 35 40 + ‘ II‘ 45 50 55 58 I60....65Ill,70 ।........... +H— II’ 75 80 85 90 95 86

Abundance #4069:2-Buten-1-ol, 3-methyl- ‘It "74I 1 1 1 7h 4.20 4.40 4.60 4.80 5.00 m/ z 43.10 52.70%

5000 27 39 53

31 68

m/z-> 49 0 1' i'11' i' 1 '71 1 1 11TT fi rM ' I ITTT 20 25 30 35 40 45 50 55 59 1111111" 1111 60 65 70 —TPPTT 75 80 86

85 90 95 -AAAAa 4.20 4.40 4.60 4.80 - 5.00

)0739.D SCAN508.M Thu Jan 17 08:17:51 2002 Page 4

NYC-WTC_000051974