GCMS results for sample AE00737, Jan 29 2002

NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02JAN16\00737.D Vial: 5 . Acq On : 16 Jan 2002 6:26 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 2-Buten-l-ol, 3-methyl- $$ ... Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

4.62 0.15 ug/L 56098 1,4-Dichlorobenzene-d4 9.71

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Buten-l-ol, 3-methyl- $$ .gamm... 86 C5H10O 000556-82-1 52 2 2-Buten-l-ol, 3-methyl- (CAS) $$... 86 C5H10O 000556-82-1 52 3 2-Buten-l-ol, 3-methyl- 86 C5H10O 000556-82-1 42 4 2-Buten-l-ol, 3-methyl- 86 C5H10O 000556-82-1 42 Abundance Scan 109 (4.618 min): 00737.D (-) m/z 71.05 100.00% 41 71 88 53 57 5000 14 68 85 __ N.A), 4.20 4.40 4.60 4 80 5.00 49 Of ■ i ■''' i ■ ■ ■' i' 11PP 1it mPT m/z 41.10 97.90% ■n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4067:2-Buten-1-ol, 3-methyl- $$ .gamma., gamma-Dimethyl... 7h

5000 A ,A 53 4.20 4.40 4.60 4.80 5.00 27 86 31 67 m/z 88.00 67.61% 59 1111 ■ ■ i ■ ■1 ■ i ■ ■ Ot • • i > ■ ■ ■ i • ■ ■ i' ■ ■' i ■ ‘ ■11 ■ ■ ■ ‘ i ■ ■ • ’ 11 ■ . ................ 'I1 1 ■ ■ i ■ ■ ■ • i •

n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4075: 2-Buten-1-ol, 3-methyl- (CAS) $$ Prenol $$ 2-METHYL... 7h 41 । 1 । 1 ' i ■ ■ ■ . I . 4.80 5.00 1 4.20 4.40 4.60 5000 m/z 57.10 54.96% 53 86 67 A 83. n/z-> 01 ' i ■ ■ ■' i' ■ ■ ■ i ■ ■ ■ • i ■'' ■ i 20 25 30 35 40 II..... Ial ■' i''' ■ i' 197 .............. ■ ■ ■ 11»■ ■ i ■ • > • i > • 45 50 55 60 65 70 75 80 85 90 95 Abundance #4069: 2-Buten-1-ol, 3-methyl- ■ i ■ ■ ■ ■ । • 7h 4.20 4.40 4.60 4.80 5.00 m/z 53.10 49.39%

5000 27 39 53

31 68 86 49 59 l ■ • I > •. > 11 > 1111 ■'' ।" 11 ■ 0 ■ ■ r '' ■ i ■ 111 " I " 111'r > I " 111" > 111 IIt n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 4.20 4.40 4.60 4.80 5.00

10737.D SCAN508.M Thu Jan 17 08:17:39 2002 Page 4

NYC-WTC_000051937