GCMS analysis results for sample AE00108, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN25\00108.D Vial: 6 Acq On : 25 Jan 2002 2:18 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 2-Buten-l-ol, 3-methyl- Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T. 4.62 0.09 ug/L 40548 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Buten-l-ol, 3-methyl- 86 C5H10O 000556-82-1 38 2 2-Buten-l-ol, 3-methyl- (CAS) $$... 86 C5H10O 000556-82-1 38 3 3-Penten-2-ol $$ .alpha.,.gamma.... 86 C5H10O 001569-50-2 23 4 N-HEXYL AMINE 101 C6H15N 000000-00-0 22 Abundance Scan 109 (4.618 min): 00108.D (-) m/z 71.10 100.00% 41 71 57 88 5000 53 101 n.'.-4.40 .1.4 4.60 MArAs., m/z-> — M 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 i1"1 i — i • • ■ * i ” I . | <T i l | 4.20 m/z 41.10 4.80 5.00 87.50% Abundance #4069:2-Buten-1 -ol, 3-methyl- 71

AI ' .44.AAM 5000 27 39 53 4.20 4.40 4.60 4.80 5.00 m/z 57.10 68.04% 86

lz-> 111111111 ‘ i- ‘ ‘ I ‘ • p-rrrp-rrrp-r 1.59.. Hli. tmm 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #4072:2-Buten-1 -ol, 3-methyl- (CAS) $$ Prenol $$ 2-METHYL... 71 1.A, r.> 4.20 4.40 4.60 4.80 5.00 5000’ 27 39 53 m/z 88.00 60.20%

miz-> 1 < 1111' I • m i" " I'1" I" 59 661 T| r 11 q n, i । HI 11 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 tmmP 86

Abundance #4047:3-Penten-2-ol $$ alpha., gamma.-Dimethylallyl alco... s ri r 1 I . 43 71 4.20 4.40 4.60 4.80 5.00 m/z 43.10 41.85% 5000 27 53

m/z—> 1111"11' r 38 i TTTTTTT 58 ....... II- 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 . 86 ’ 4.20/At YWA-P4 4.40 4.60 4.80 5.00

00108.D SCAN508.M Mon Jan 28 09:49:59 2002 Page 5

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