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GCMS analysis results for sample AE00108, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.

NYC-WTC_000050754–000050773

Folder label: “GCMS X 1/4/02 A 1/25/02

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Scanned page image, NYC-WTC_000050761
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN25\00108.D Vial: 6 . Acq On : 25 Jan 2002 2:18 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 2(3H)-Furanone, 5-ethyldihy... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R. T.

4.24 0.11 ug/L 50058 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2(3H)-Furanone, 5-ethyldihydro- ... 114 C6H10O2 000695-06-7 33 2 Pentane, 2-bromo-4-methyl- 164 C6H13Br 030310-22-6 33 3 Methacrylamide $$ 2-Propenamide,... 85 C4H7NO 000079-39-0 28 4 (Z)-3-[[(1'-Oxacyclohex~2'-yl)ox. .. 254 C15H26O3 076481-04-4 23 Abundance Scan 76 (4.241 min): 00108.D (-) m/ z 85.10 100.00% 41 85

5000 60 —A 3.80 4.00 4.20 4.40 4.60 _ .... . ,11,47.1,1 . ............. Ill ................................. m/z 41.10 87.10% /z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #14904:2(3H)-Furanone, 5-ethyldihydro- (CAS) $$ .GAMMA.-N... 85

5000 29 AA.A SAMN. 3.80 4.00 4.20 4.40 4.60 42 56 m/z 43.10 57.40% 15 70 miz-> 4P .n ' op 1 1 I ' ' ’ 1 T ' 1 p.r .r.’.1.'. , । 10 20 30 40 50 60 70 80 90 100 110 120 113 ' 1 i b ■ 1 1 I ' 1 1 1 I ' 1 1 1 1 1

Abundance #63838: Pentane, 2-bromo-4-methyl- 43

3.80 4.00 4.20 4.40 4.60 85 5000 m/z 39.10 32.52% 27 69 15 _1 .... | 371 ■.n.■.1,57.Ir.,.- —I I ■ I • * < । | ‘ ‘ 107 ■ • i ■ ■ ■ ' i ' 1 ' 1 i b ''I mz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #3602: Methacrylamide $$ 2-Propenamide, 2-methyl- $$ .alph... 41 85 3.80 4.00 4.20 4.40 4.60 m/ Z 60.10 28.40%

5000- 69

m/z—> - 10 20 30 40 153 50 ...... 60 70 < I 1 ' I ' I ' ' ■ > I ' 80 90 100 • 1 i 1 1 1 1 i 1 110 120 ......... I ' 1 1 ' I1' 3.80 4.00 4.20 ' '"T TTTTr 4.40 .4.60

00108.D SCAN508.M Mon Jan 28 09:49:59 2002 page 4

NYC-WTC_000050761

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NYC-WTC_000050761Source: NYC Law Department, mirrored locally

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