GCMS analysis results for sample AE00106, Feb 2002

NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02JAN25\00106.D Vial: 5 Acq On : 25 Jan 2002 1:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 5 1-Hexene, 6-bromo- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 4.83 0.20 ug/L 88598 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Hexene, 6-bromo- 162 C6HllBr 002695-47-8 12 2 Cyclobut-l-enylmethanol 84 C5H80 000000-00-0 10 3 4-Pentenal (CAS) $$ 4-Pentenal- 84 C5H80 002100-17-6 10 4 Formamide, N-(cyanomethyl) - 84 C3H4N20 005018-27-9 9 Abundance Scan 128 (4.835 min): 00106.D (-) m/z 84.00 100.00% 84 55 5000 39

4.40 4.60 4.80 5.00 5.20 TT Ll 69 m/z 55.10 63.67% "It ■ i ■' ■ ■ i1' ■' i' i ■ ■ ■ ■ i ■'' ■ । ' i ■ ■ ■ ■ i l11111' ■ ‘ ■ i ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #61497:1-Hexene, 6-bromo- _........... 41 55

83 A 5000 27 67 4.40 4.60 4.80 5.00 5.20 m/ z 83.10 43.25%

n/z-> 20 ' I ' '' ' I ' '' ' I 30 40 L 50 — +1 134 I' BIT 162 ' i ■ ■ ■ ■ i

60 70 80 90 100 110 120 130 140 150 160 170 Abundance #3313: Cyclobut-1-enylmethanol 55 83 4.40 4.60 4.80 5.00 5.20 27 39 5000 m/z 59.10 40.42%

1 66 1 ' i,1111 ,11. ......... 1111111 TIT i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i V n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #3205:4-Pentenal (CAS) $$ 4-Pentenal- . /MV... 55 4.40 4.60 4.80 5.00 5.20 m/z 39.10 37.87% 83 27 39 5000

— n/z-> pul... 11 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 4 40 4.60 4.80 5.00 5.20

00106.D SCAN508.M Mon Jan 28 09:49:53 2002 Page 7

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