GCMS analysis results for sample AE00106, Feb 2002

NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02JAN25\00106.D Vial: 5 Acq On : 25 Jan 2002 1:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 4 2-Buten-l-ol, 3-methyl- $$ ... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 4.63 0.10 ug/L 43655 1,4-Dichlorobenzene-d4 9.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Buten-l-ol, 3-methyl- $$ .gamm... 86 C5H10O 000556-82-1 38 2 Butanoic acid, 2-methyl-, methyl... 116 C6H1202 000868-57-5 38 3 2-Buten-l-ol , 3-methyl- 86 C5H10O 000556-82-1 38 4 Butanoic acid, 2-methyl-, methyl... 116 C6H1202 000868-57-5 38 Abundance Scan 110 (4.629 min): 00106.D (-) m/z 41.10 100.00% 41 57 71 88

5000

101 Al A 4.20 4.40 AA 4.60 N NA 4.80 500

n/z-> ■ r •' ■ i" 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 +84l ■ I " " r ■ ■ ■ i '■r'"r m/z 71.10 97.46% Abundance #4067:2-Buten-1 -ol, 3-methyl- $$ gamma., gamma.-Dimethyl... 71

5000 53 4.20 4.40 —AA 4.60 4.80 5.00 27 86 m/z 88.10 96.37% ... ■ ■ i ■ ■ ■ ■ i' . ............. 1 " ■' " i ■■ T‘ i i ■■ i

n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #16439: Butanoic acid, 2-methyl-, methyl ester (CAS) $$ Me... 57 88

4.20 4.40 4.60 4.80 5.00 41 m/z 57.10 88.65% 5000

101 69 nz-> i" ।" I H m 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 " ■ i" " i'

Abundance #4068:2-Buten-1 -ol, 3-methyl- I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' 71 4.20 4.40 4.60 4.80 5.00 m/z 39.10 43.87%

5000 53 27 86

m/z-> i" i 66 H1" i1111 r" " r11111 I’’’’ I T’ llll""l"lll + r ' "i"r"■ i 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 TT 4.20 4.40 4.60 4.80 5.00

30106.D SCAN508.M Mon Jan 28 09:49:53 2002 Page 6

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