GCMS analysis results for sample AE00470, Jan 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\00470.D Vial: 4 Acq On : 15 Jan 2002 12:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 1 2-Buten-l-ol , 3-methyl- Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 4.63 0.12 ug/L 38611 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Buten-l-ol, 3-methyl- 86 C5H10O 000556-82-1 38 2 Butanoic acid, 2-methyl-, methyl... 116 C6H1202 000868-57-5 38 3 Butanoic acid, 2-methyl-, methyl... 116 C6H12O2 000868-57-5 23 4 Butanoic acid, 2-methyl-, methyl... 116 C6H12O2 000868-57-5 23 Abundance Scan 110 (4,630 min): 00470.D (-) m/z 41.10 100.00%| 41 57 71 88

5000 53 101 AAANA 4.20 4.40 4.60 4.80 5.00 0 " i" U ।1 “ ■ r11" ।'1 TTT 'I...... I ■' i1 r" i" " i ■" । TTTH "| •Ir m/Z 71.10 98.39% /z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #4074: 2-Buten-1-ol, 3-methyl- 71

5000 39 53 8 N, I \ 4.20 4.40 4.60 4.80 5.00 27 86 m/ Z 88.00 91.47%|

n/z-> Of TTTTTT’ TPT H H Imi " ' I 1" i "1111" 111'" i “ ■' r 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #16434: Butanoic acid, 2-methyl-, methyl ester $$ Butyric ... 57 88

4,20 4.40 4.60 4.80 5.00 5000 m/z 57.10 86.91% 27 101 69 0 TPTWTLTTPTTTTTT +ri i i rp i 11 ] i i I i । i i i i । i i n + — —mp i ■''' i n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #16439: Butanoic acid, 2-methyl-, methyl ester (CAS) $$ Me... 57 88 4.20 4.40 4.60 4.80 5.00 m/z 43.10 48.62% 41 5000

101 69 0 TU’PT " r "11" " i mm*m4 nmmm — — AM m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 4.20 4.40 4.60 4.80 5.00

0470.D SCAN508.M Wed Jan 16 08:13:50 2002 Page 3

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