GCMS analysis results for sample AE00558, Jan 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\00558.D Vial: 2 Acq On : 15 Jan 2002 2:21 pm Operator: , Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 1 1-Hexene, 6-bromo- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

4.86 0.15 ug/L 41913 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Hexene, 6-bromo- 162 C6HllBr 002695-47-8 9 2 5-Hexenal oxime 113 C6H11NO 057606-82-3 9 3 1-Hexene, 6-bromo- (CAS) $$ 6-Br... 162 C6HllBr 002695-47-8 9 4 1-Hexene, 6-bromo- 162 C6HllBr 002695-47-8 9 Abundance Scan 130 (4.858 min): 00558.D (-) m/ z 83.95 100.00% 84 55 41 5000

4.60 4.80 5.00 5.20 O' i111' i111' r 1,1 _ ‘IT ' I' ' ' • I ' I • 1 I ' • I ‘ I ' i' ■ ■ ■ i' ■1 ■ 111'11 m/z 55.10 69.28% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #61497:1-Hexene, 6-bromo- 41 55

83 ......... .......................... ........... 5000 27 67 4.60 4 80 5.00 5.20 m/z 41.10 53.27%

n/z-> O-TT 20 30 40 .. mi....... 50 60 70 1 ■ ■ i• • • > i• ■ •• i >• ■ >i 80 90 100 110 120 134 I'1'............. 130 140 150 160 170 162 111111 ri

N Abundance #14234:5-Hexenal oxime 41 55 4.60 4.80 5.00 A 1 ’I 11 11 5.20 5000 27 m/ z 83.00 36.93%

113 O' । ■ ■ ■ ■ । ■ ' I' 1 '' I '' ’ ’ I ‘ ' 'I' i • ■ ■ ■ । ‘II i'' ■ ■ i'' ■11 ■ ‘ ■ ■ i m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #61499:1-Hexene, 6-bromo- (CAS) $$ 6-Bromo-1-hexene $$ 1-... 41 55 4.60 4 80 5.00 5.20 m/ Z 39.10 35.77% y 83 5000 67 27

0 > । ■11•। '| ।... ।. ■ i ■ ■ ■ ■ i ■' ■ • i TIB i ■ • ■ ■ i 162 I ' '' ■ I' '' ' I' ' '' I ' ■ ' ■ I 11'' I' ■

m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 4.60 4.80 5.00 5.20

00558.D SCAN508.M Wed Jan 16 08:14:00 2002 Page 3

NYC-WTC_000051720