GCMS analysis results for sample AE00615, Feb 2002

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Laboratory report showing GCMS analysis results for sample AE00615 conducted on February 1, 2002.

NYC-WTC_000051624–000051641

Folder label: “GCMS X 1/9/02 A 1/29/02”

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NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02JAN29\00615.D Vial: 4 - Acq On : 29 Jan 2002 5:09 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 6 1,6-Heptadien-4-ol Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

5.71 0.07 ug/L 34583 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,6-Heptadien-4-ol 112 C7H120 002883-45-6 39 2 Butenol, methyl- 86 C5H10O 060766-00-9 9 3 Butane, 1-bromo-2-methyl- (CAS) ... 150 C5HllBr 010422-35-2 9 4 2-Butene, 1-methoxy-, (E)- 86 C5H10O 010034-14-7 9 Abundance Scan 205 (5.714 min): 00615.D (-) m/z43.10 100.00% 43 71

5000

' ■ 1 "I ■ ' r 1 P 1 ■ ‘ ■ ■ C 'I 51 84 5.40 5,60 5.80 6.00 ■' i ■ ■r ■ i' ■ ’' i1 "'I'1........................... i ri " r' " ITTTru i m/z 71.10 92.40% nz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #13655:1,6-Heptadien-4-ol 43 7h

5000 T-r-p-r-r-r-p-r TT 5.40 5.60 5.80 6.00 27 m/ z 41.10 80.90% 53 । 11 ■ i '' TIT 1 79...94 .................... T 11" i111' r " 1111" i111•।< <.11,,,।p,i,P niz-> 10 20 30 40 50 60I 70 80 90 100 110 120 130 140 150 Abundance #4093: Butenol, methyl- 43 71 PTIr 'I ■ ■ < * । ■ ■ • ■ । 5.40 5.60 5.80 6.00 5000 59 m/ z 69.10 48.73% 27 15 .................. ........ ,,511., ■■i ■' ■ ■ i11 ■ ■ i' ■ ■' 11 ■' ■ i' ■ ■11'1 TTT ...... ■ I .. ............. ...................... >r • • i ■ ■ • • i • > ■ ■ i ■ ■1 ■ i ■ ■ • • । ■ i ■ ■ ■ • i n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #45644: Butane, 1-bromo-2-methyl- (CAS) $$ 1-Bromo-2-methy... nm/g MPe . . , । 41 71 5.40 5.60 5.80 6.00 m/z 39.10 47.49%

5000 57

m/z—> ' ‘ 11''' I''1 1. •'' ■ i1 ■ ■11 ■ ■111 • ■'' i ■' ■ ■ i''' ■.' 10 20 30 40 50 60 150 i'1 ’ ■. ■ ■ ■ ■. 70 80 90 100 110 120 130 140 150 i ■ ■ ■ ■ i rp-n —A 5.40 5.60 5.80 6.00

00615.D SCAN508.M Wed Jan 30 09:02:21 2002 Page 8

NYC-WTC_000051635

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