GCMS analysis results for sample AE03251, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03251 conducted on March 15, 2002.

NYC-WTC_000006206–000006225

Folder label: “GCMS X 2/12/02 A 3/01/02”

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Data File : C:\MSDCHEM\1\5973N\02MAR01\03251.D Vial: 6 - Acq On : 1 Mar 2002 8:07 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 6 2-Furanmethanol, tetrahydro... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 5.01 0.17 ug/L 70252 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Furanmethanol, tetrahydro- (CA... 102 C5H10O2 000097-99-4 64 2 3-Buten-2-ol, 2-methyl- (CAS) $$... 86 C5H10O 000115-18-4 50 3 Butenol, methyl- 86 C5H10O 060766-00-9 50 4 3-Buten-2-ol, 2-methyl- (CAS) $$... 86 C5H10O 000115-18-4 43 Abundance Scan 145 (5.011 min): 03251 .D (-) m/z 71.00 100.00% 43 7h

5000 55 59

67 _AA 4.60 4.80 5.00 5.20 5.40 m/z-> Or .Jill.. 51I...1/7.1 11 1 " ‘ I " '''T1 ' I ! | I I I I | I I I I | 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 J ' I “ “ I'11111 " 1 Prr 'I m/z 43.10 83.11% Abundance #9384: 2-Furanmethanol, tetrahydro- (CAS) $$ Tetrahydrofur... 7h 43

5000 27 AAAAAAAWAAA 31 4.60 4.80 5.00 5.20 5.40 m/z 41.10 73.30% 53

n/z-> 5 Or '■'I ‘ 1+L761.4 ‘ 11 n .. ।. .. . ।. 37 ’ 1- 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Frrj 11111111111111111111

Abundance #4081: 3-Buten-2-ol, 2-methyl- (CAS) $$ 2-Methyl-3-buten-2... Th MWAMW. , A , A , I 1 1 11 1 11 1 1 1 111 1 11 1 ’ I ' ' 43 4.60 4.80 5.00 5.20 5.40 5000 m/ z 69.10 43.10% 59 27 31 53 67

miz- > 5 0b '11" " i " " i" ■11 ■ - ■ ■ 11 ■ ■11 ■ ■'11' l

10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 .......... ^I" H Abundance #4093: Butenol, methyl- 43 71 4.60 4.80 5.00 5.20 5.40 m/z 59.10 36.60%

5000 59 27 15 31 53 Ob '11 " " i" " i' ’ T ■11 ‘ ■ i" -HH mlil 186 671 N, /z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 4.60 4.80 5.00 5.20 5.40

3251.D HP022102.M Mon Mar 04 12:33:48 2002 Page 8

NYC-WTC_000006217

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