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GCMS analysis results for sample AE00027, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00027 analyzed on February 7, 2002.

NYC-WTC_000050735–000050753

Folder label: “GCMS X 1/4/02 A 1/25/02

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Scanned page image, NYC-WTC_000050744
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document -- XT----

Data File : C:\MSDCHEM\1\5973N\02JAN25\00027.D Vial: 3 , Acq On : 25 Jan 2002 4:47 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ***************************************************************** ** * * Peak Number 4 THIOPHENE-D3 Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 4.24 0.10 ug/L 41203 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 THIOPHENE-D3 87 C4HD3S 000000-00-0 9 2 2-OXO-PROPIONAMIDE 87 C3H5NO2 000000-00-0 9 3 THIOPHENE-D1 85 C4H3DS 000000-00-0 9 4 Methacrylamide 85 C4H7NO 000079-39-0 9 Abundance Scan 76 (4.241 min): 00027.D (-) m/z 87.10 100.00% 4B 87

5000 39 51 55 59 T T. 1 'T' 11 3.80 4.00 4.20 4.40 4.60 ■ I' ■111 ’ 84 m/z 43.10 98.30% T /z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #3150: THIOPHENE-D3 87

5000 46 59 —m/z A 3.80 •4.00 41.10 4.20 4.40 4.60 89.67% ........................ 34.............. 49 ----- +HT " 1111111' n/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4310:2-OXO-PROPIONAMIDE 43 87 AAAALAAL 3.80 4.00 4.20 4.40 4.60 5000 m/z 85.00 75.72%

niz-> 15 27 ■i■ "111''1111 lb । " "11 20 25 30 35 40 +6 —52 57 NPTTTT ' IH " i" ■' i" " i ■" ■ r " ' i" " i ■ 45 50 55 60 65 70 75 80 85 90 95 ----- Abundance #3148: THIOPHENE-D1 85 3.80 4.00 4.20 4.40 4.60 m/z 89.00 70.40% 5000 45 58 40

..... 3437..., +HTT 49 npl ■ p " 11'11 b i ’ ■ " r " ' i" ' । +.FTTTI.rT.r 1 i ■ b 1 1 i ■ 1 ■ । i ■ ■ miz-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.80 4.00 4.20 4.40 4.60

00027.D SCAN508.M Mon Jan 28 09:49:29 2002 Page 6

NYC-WTC_000050744

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NYC-WTC_000050744Source: NYC Law Department, mirrored locally

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