GCMS analysis results for sample AE00101, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02JAN23\00101.D Vial: 4 Acq On : 23 Jan 2002 5:25 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 THIOPHENE-DI Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

4.24 0.17 ug/L 56896 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 THIOPHENE-DI 85 C4H3DS 000000-00-0 40 2 3-Methyl-2,3-epoxybutanal 100 C5H802 000000-00-0 36 3 Pentane, 2-bromo-4-methyl- 164 C6H13Br 030310-22-6 36 4 2(3H)-Furanone, 5-ethyldihydro- ... 114 C6H10O2 000695-06-7 36 Abundance Scan 76 (4.241 min): 00101 .D (-) m/z 85.00 100.00% 85 41

5000

55, 60 3.80 4.00 NNA..A, 4.20 4.40 4.60 01 1 I 1 ' 1 1 I ' 1 1 ■ t 1 ■ ■ • I • ■ । ■ 1 i ■ • ll.l.............. m/z 41.10 70.89% iz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3148: THIOPHENE-D1 85

5000 45 58 A A 3.80 4.00 4.20 4.40 4.60 ' N 40 m/z 43.10 56.77%

0TT ................. , - nz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #7969:3-Methyl-2,3-epoxybutanal 41 85

3.80 4.00 4.20 4.40 4.60 5000 m/z 60.00 30.50% 60

, 100 0-t I | ji H • * I * J * * * * j i i I i J i ! rn i i । I । । । i I । 1’14 । i । i । । । । i । । । miz-> 10 20 30 40 50 60 70 80 90 1(X) 110 Abundance #63838: Pentane, 2-bromo-4-methyl- i ■ • ■ ■ i ■ 1 ■ ' i ■ 1 ■ ■ i ■ ‘ ■ i ■ ■ 43 3.80 4.00 4.20 4.40 4.60 m/z 39.10 21.29% 85 5000 27 69 15 57 1.... 1 , 371 0 ■ ■ i • ' ■ ■ i ■ ■ ■ ■ i ■ ......... I|.......... —84 ---19— [*’’I*4’*I’+-*I***’ i ■ ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 3.80 4.00 4.20 4.40 4.60

00101.D SCAN508.M Thu Jan 24 09:57:13 2002 Page 3

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