Quality control report for GCMS analysis of sample AE00277 showing surrogate recovery data from January 10, 2002.
NYC-WTC_000050838–000050855Folder label: “GCMS X 1/7/02 A 1/9/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Data File : C:\MSDCHEM\l\5973N\02JAN09\277.D Vial: 2 Acq On 9 J an 2002 6:59 pm Operator: Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 8 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
22.28 0.18 ug/L 138396 Phenanthrene-diO 22.63
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 72 2 1,4-Dimethyl-3,5-propanobicyclo [... 192 C13H20O 000000-00-0 49 3 2-Imidazolidinone, 1-methoxy-3-p... 192 C10H12N2O2 052420-43-6 47 4 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 42 Abundance Scan 1656 (22.280 min): 277.D (-) m/z 192.10 100.00% 192
5000
′′′ 41 54 —70 82| 96 120 146 160 11 22.00 22.20 22.40 22.60 0 i MIPTTT+i T HT , I I ] 11 i, ।. ITi TT ■ 11> ■. r]. ..... ..... +—..... 111...... m/z 96.10 16.30% n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424: 3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192
5000 ----- -A 22.00 22.20 22.40 22.60 164 m/z 191.10 13.86% 138 oR --TT 11n m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103601:1,4-Dimethyl-3,5-propanobicyclo[2.2.2]octan-2-one 107 192 ■ 1 I 1 ’ 1 ■ I I1' 119 159 93 22.00 22.20 22.40 22.60 5000 m/z 146.10 11.97% 132 145 174
m/z-> Ofr 30 40 ' i " " I " " I " " r " ■ i' 50 60 " I " " I " " I" " " " I ■ ‘ i " " i " 70 80 90 100 110 120 130 140 150 160 170 180 190 200 "It "l""l 1 Abundance #102450: 2-lmidazolidinone, 1-methoxy-3-phenyl- ----- 106 192 22.00 22.20 22.40 22.60 m/z 82.00 11.68% 77 119 162 5000 42 56
134 PPP । । MA 0109.9 I m/z-> O- -i-rp- ’11’1 ■ 111" l1 ■ ■ ■ i ■1 ■ ■ i ■ ■ ■ ■ i ■ 1' ‘ P ■ ■ ■ । 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 TT’I 22.00 22.20 22.40 22.60
277.D SCAN508.M Thu Jan 10 11:51:37 2002 Page 10
NYC-WTC_000050852
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NYC-WTC_000050893
Laboratory record documenting GCMS surrogate recovery data for sample AE00280 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050912
Laboratory record documenting GCMS surrogate recovery data for sample AE00281 analyzed on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050875
Laboratory record documenting GCMS surrogate recovery data for sample AE00279 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050932
Laboratory record documenting GCMS surrogate recovery data for sample AE00282 analyzed on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051755
GCMS analysis log for sample AE00561 showing surrogate recovery and unknown compounds detected on January 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050856
Laboratory record documenting GCMS surrogate recovery data for sample AE00278 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050963
Laboratory record documenting GCMS surrogate recovery data for sample AE00316 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050977
Laboratory record documenting GCMS surrogate recovery data for sample AE00317 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051727
Laboratory report showing GCMS analysis results for sample AE00559 conducted on January 17, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051685
Laboratory report showing GCMS analysis results for sample AE00365 conducted on January 17, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051586
Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050948
Laboratory record documenting GCMS surrogate recovery data for sample AE00310 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000050813
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050814
Fragmented page from a DEP laboratory record showing method parameters and sample data fields for January 7-9, 2002 testing.
Filed in the same folder
NYC-WTC_000050817
Technical form detailing GCMS analysis results for sample AE00277 listing detected compounds and concentrations from January 9-10, 2002.
Filed in the same folder
NYC-WTC_000050821
Reference report for GCMS analysis of sample AE00277 listing compound names and qualifier values from January 9-10, 2002.
Filed in the same folder
NYC-WTC_000050825
Blank analysis report for GCMS of sample AE00277 showing compounds below method detection limits from January 10, 2002.
Filed in the same folder