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GCMS results for sample AE00468, Jan 18 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00468 with surrogate recovery data on January 18, 2002.

NYC-WTC_000051318–000051335

Folder label: “GCMS X 1/8/02 A 1/10/02

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Scanned page image, NYC-WTC_000051329
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN10\00468.D Vial: 5 Acq On 10 Jan 2002 6:07 pm Operator: Sample 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ******************************************************** ****** ** * * *** Peak Number 6 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.16 ug/L 84948 Phenanthrene-dl0 22.63 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 72 2 2-CYANOCARBAZOLE $$ 9H-Carbazole... 192 C13H8N2 057955-18-7 72 3 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 4 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 58 Abundance Scan 1656 (22.280 min): 00468.D (-) m/z 192.10 100.00% 192

5000

96 | T > i I | i I

146 160 22.00 22.20 22.40 22.60

m/z-> 44 66 82 0 ' ' I 1 1 ' 'V-+Hr . 11111 T . । 118 1111 i 11 TTTH I ■11" 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 l m/z 193.10 16.86% Abundance #103424: 3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192

5000 22.00 22.20 22.40 22.60 96 164 m/z 96.10 16.20% 138 0- " i11" i' ----- 111........... 11, 'i'" if ' ।' 11' 111' ■ m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103420: 2-CYANOCARBAZOLE $$ 9H-Carbazole-2-carbonitrile (CAS 192 A 22.00 22.20 22.40 22.60 5000 m/z 191.10 15.74%

96 164 0....... T ' i1 ‘'11' " 111 i'''' i' ■' ■ i .... 138........1.........1 TT‘1 m/z--> Abundance 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192 M TII T 22.00 22.20 22.40 22.60 m/z 146.10 15.23% 5000

96

m/z-> 88 , 139 152 165 +4—PHmH 0 ' ' I ‘ 1 1 * mTu I | I । । । | fM I | I I I I Dr’ t 11■r'11■ ■ ■■ i111 'i ■ ■ ■ ■ ।1 ■ ■ ■ i ■ 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 176 L -A 22.00 22.20 22.40 22.60

90468.D SCAN508.M Fri Jan 11 10:08:43 2002 Page 8

NYC-WTC_000051329

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NYC-WTC_000051329Source: NYC Law Department, mirrored locally

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