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GCMS results for sample AE00468, Jan 18 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00468 with surrogate recovery data on January 18, 2002.

NYC-WTC_000051318–000051335

Folder label: “GCMS X 1/8/02 A 1/10/02

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Scanned page image, NYC-WTC_000051328
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN10\00468.D Vial: 5 Acq On 10 Jan 2002 6:07 pm Operator: • Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCJ\N508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 5 5-Nitro-2-furaldoxime $$ 2-... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 18.73 1.03 ug/L 529744 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 5-Nitro-2-furaldoxime $$ 2-Furan... 156 C5H4N2O4 000555-15-7 40 NO 2 CYSTEIC ACID THIOHYDATOIN 210 C4H6N204S2 000000-00-0 36 3 Pyrazole, 3-(p-chlorophenyl)-5-m. .. 192 C10H9C1N2 017629-27-5 9 Mn(ok 4 Benzene, 1-bromo-3 -chloro- 190 C6H4BrCl 000108-37-2 9 Abundance Scan 1345 (18.730 min): 00468.D (-) m/ z 64.00 100.00% 64 192

5000 128 1 ' i ■ ■ ’ “’ I > I । । | । । i r | i > . . । 96 18.40 18.60 18.80 19.00 0 44 I 76 " ] * 1 ' r I ' " ' I 1 ‘I ■ i ■ ............. 162 180 TPWTTTTTTTTTTTTTTTTTT 4p m/z 191.80 98.94% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #54546: 5-Nitro-2-furaldoxime $$ 2-Furancarboxaldehyde, 5-... 33 64 54 8 126 138 5000 108 156 18.40 18.60 18.80 19.00 80 m/z 127.90 32.04% 96 0 I " ’' I TTTT —L H I " * ’I I' " ’ I 11" 'T' 111111111 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #129028: CYSTEIC ACID THIOHYDATOIN 48 64 A— ■I 1 ' 1 ‘ I 18.40 18.60 18.80 19.00 5000 m/z 193.80 25.16% 128 76

m/z—> 0 " i'1" i T‘r MX™ 'I" " । 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ।।" i" " i ■" ■ i" ■11"

Abundance #102437: Pyrazole, 3-(p-chlorophenyl)-5-methyl- 192 18.40 18.60 18.80 19,00 m/z95.90 14.57% 5000

42 75 128

0 r . I.. r "' i I itsyoallane 151.... 177...II 111 TT 111111111 'T7'" 111111" " I" ...... /, I m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 18.40 18.60 18.80 19.00

30468.D SCAN508.M Fri Jan 11 10:08:43 2002 Page 7

NYC-WTC_000051328

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NYC-WTC_000051328Source: NYC Law Department, mirrored locally

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