Laboratory report for sample AD31675 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
NYC-WTC_000050294–000050316Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02JAN24\31675A.D Vial: 2 Acq On : 24 Jan 2002 12:31 pm Operator: Sample : 508scan; re-inj Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 5-Nitro-2-furaldoxime $$ 2-... Concentration Rank 12
R.T. EstConc Area Relative to ISTD R.T.
21.62 0.10 ug/L 68310 Phenanthrene-dl0 22.65
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 5-Nitro-2-furaldoxime $$ 2-Furan... 156 C5H4N2O4 000555-15-7 40 2 Propanoic acid, 2-chloro- 108 C3H5C102 000598-78-7 9 3 Ethane, chloro- (CAS) $$ Chloroe... 64 C2H5C1 000075-00-3 7 4 Ethane, chloro- (CAS) $$ Chloroe... 64 C2H5C1 000075-00-3 7 Abundance Scan 1598 (21.618 min): 31675A.D (-) m/z 63.90 100.00%
5000 64
130 160 192 Pww"w 96 49 21.20 21.40 21.60 21.80 22.00 ' Tmmag ‘ I'''' I'' ‘' I I' ■'' 11' ‘' I I' “ ' I 1 ’ •“ l ’ * • ‘ I ‘‘I‘ m/z 191.80 48.24% miz-> 2030405060 70 8090 100 110 120130 140 150 160170180 190 200 Abundance #54546:5-Nitro-2-furaldoxime $$ 2-Furancarboxaldehyde, 5-... 33 64 MWW 54 5000 126 138 21.20 21.40 21.60 21.80 22.00 108 156 80 m/z 159.80 31.30% 96 I.... 1.... 1.... j ‘I"3 I•*’‘I I““I T I • • •' l T" n/z-> 20 30 40 50 60 70 80 90 100 110120130 140 150 160 170180190 200 Abundance #11024: Propanoic acid, 2-chloro- 27 64
21 20 21.40 21 60 21 80 22.00 5000 45 m/z 129.90 27.95%
73 108 ‘188 . 11'... t।j... 11।।।।t......... t....,. n/z-> 20 30 40 50 60 70 80 90 100 110 120130 140 150 160 170 180 190 200 Abundance #927: Ethane, chloro- (CAS) $$ Chloroethane $$ Ethyl chlor... T T T T 64 21.20 21.40 21.60 21.80 22.00 m/z 65.95 26.72% 5000
35 49 MMA nMMpn vfz-> lm ।j।।।।j.... j.... j।।. 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 1 i ■ ■ ■ ■ i ■ • 21.20 21.40 21.60 21.80 22.00
31675A.D SCAN508.M Thu Jan 24 15:25:30 2002 Page 9
NYC-WTC_000050310
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NYC-WTC_000050276
Laboratory report documenting GCMS analysis of sample AD31674 with detection of unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050317
Laboratory report for sample AD31676 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050258
Laboratory report documenting GCMS analysis of sample AD31664 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051024
Laboratory report documenting GCMS blank analysis to verify system cleanliness during January 8-10, 2002 testing.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050205
Laboratory report documenting GCMS analysis of sample AD31647 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050222
Laboratory report documenting GCMS analysis of sample AD31645 with detection of unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050397
Laboratory report for sample AE00698 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050024
Laboratory report showing GCMS analysis of sample AD31671 including unknown compounds and surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050354
Laboratory report for sample AE00100 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050370
Laboratory report for sample AE00101 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018830
GCMS report for sample AD28861 showing detection of unknown compounds and surrogate recovery data.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003981
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
2 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000050177
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050178
Instrument log sheet recording sample counts and operational parameters for GCMS Method 508 analysis in January 2002.
Filed in the same folder
NYC-WTC_000050180
Calibration report for GCMS analysis of sample AD31647 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000050184
Reference scan data for GCMS analysis of sample AD31647 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000050189
Blank analysis report for GCMS testing of sample AD31647 confirming no contamination above detection limits.
Filed in the same folder