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GCMS analysis results for sample AE00465, Jan 18 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00465 conducted on January 18, 2002.

NYC-WTC_000051222–000051235

Folder label: “GCMS X 1/8/02 A 1/10/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02JAN10\00328.D Vial: 1 Acq On 10 Jan 2002 2:49 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* 38o & Peak Number 4 5-Nitro-2-furaldoxime $$ 2-... Concentration Rank 4 Joe ) Jo Gov R.T. EstConc Area Relative to ISTD R.T. 18.72 0.27 ug/L 133065 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qua.

1 5-Nitro-2-furaldoxime $$ 2-Furan... 156 C5H4N2O4 000555-15- 42 2 Pyrazole, 3-(p-chlorophenyl)-5-m... 192 C10H9C1N2 017629-27- 3 2,4-Diamino-6-(hydroxymethyl)pte... 192 C7H8N60 000945-24-4 9 4 Benzene, 1-bromo-3-chloro- 190 C6H4BrCl 000108-37-2 9 Abundance Scan 1344 (18.718 min): 00328.D (-) “I m/z 64.00 100.00% 64 192

5000 128 ' ......... . 96 162 18.40 18.60 18.80 19.00 44 n/z—> 0 ' i''111'' ■' i' ■'11' ‘ ■11 ■'' ■ i ■ ■ ■ i " " i " " 11 ■1 ■ i ■ + 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 nponl..... m/z 191.80 89.17% Abundance #54546: 5-Nitro-2-furaldoxime $$ 2-Furancarboxaldehyde, 5-... 33 64 8 54 5000- 126 138 ’ Ti । । i । । 4 . ip rr । । । । i । । 108 156 18.40 18.60 18.80 19.00 80 m/z 127.90 27.85% 96 0 i ■'" f ‘IIT TIT -rq-m-rp-r i ■11 * i ” T-p-r 'I'"'I" ‘ ‘‘ITT m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102437: Pyrazole, 3-(p-chlorophenyl)-5-methyl- 192

18.40 18.60 18.80 19.00 5000 m/z 193.80 20.83% 42 75 128

0 ' I " '11 mm 111 | 151 I i 177 ' r " ' I" " i" " i “ " r " ■ i 11 " i" /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102009: 2,4-Diamino-6-(hydroxymethyl)pteridine $$ 6-Pteri... 7* n'l' । ।1 < 1 ITTTI’ । '■ ' ' ' । 163 192 18.40 18.60 18.80 19.00 m/Z 95.90 15.01% 5000 I 66 146 176

m/z-> 0 ' I •1 TT‘ ‘ ‘I‘‘‘‘IS‘‘IUI1‘ ............................. ...... UNUT — .. Il 121

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 134 l 18.40 18.60 18.80 19.00

>0328.D SCAN508.M Fri Jan 11 10:08:21 2002 Page 6

NYC-WTC_000051231

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NYC-WTC_000051231Source: NYC Law Department, mirrored locally

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