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GCMS results for sample AE00467, Jan 24 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00467 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051453–000051470

Folder label: “GCMS X 1/8/02 A 1/11/02

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Scanned page image, NYC-WTC_000051461
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN11\00467.D Vial: 7 Acq On : 11 Jan 2002 7:05 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 3 5-Nitro-2-furaldoxime $$ 2-... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 18.73 1.36 ug/L 758011 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 5-Nitro-2-furaldoxime $$ 2-Furan... 156 C5H4N2O4 000555-15-7 42 NO 2 Pyrazole, 3-(p-chlorophenyl)-5-m... 192 C10H9C1N2 017629-27-5 9 A 3 Benzene, 1-bromo-4-chloro- 190 C6H4BrCl 000106-39-8 9 99 4 Benzene, 1-bromo-3-chloro- 190 C6H4BrCl 000108-37-2 9 we(o" m/z 191.80 100.00%

N Abundance Scan 1345 (18.730 min): 00467.D (-) 64 192

5000 128 96 18.40 18.60 18.80 19.00 44 | 76 86 | 162 180 0 i ■' ■ ■ i'1 ■11''' ■ i "TH 41 I *'' ’ I ............... . 1... I I m/z64.00 92.90% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #54546: 5-Nitro-2-furaldoxime $$ 2-Furancarboxaldehyde, 5-... 3J 64 18 54 5000 108 126 138 156 18.40 18.60 18.80 19.00 80 m/z 127.90 32.09% 96

/z—> 0 I" " I TT 4 i ■ ■1 ■ i 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 r ■" i TT I" " I । । । . vyrri ‘I’’

Abundance #102437: Pyrazole, 3-(p-chlorophenyl)-5-methyl- 192 A

N 18.40 18.60 18.80 19.00 5000 m/z 193.80 23.25% 42 75 128

0 • > ।" i ..........posomg III 111 | 151 i i r' " i" " I 177 I " •' I JI H1 " i" m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #99524: Benzene, 1 -bromo-4-chloro- 192 18.40 18.60 18.80 19.00 m/z 95.90 15.47% 111 5000 75 50 i 96 0 1■11 ■ ■■ i" ........ / ! | I I I ! | I I1! I | I I > I | ++ 130 i■' "I■ i "" r ' ■'r" 'r ■ "i "i" • ■ i • ■ p • ' ' I 1 1 ‘ ' I ' ' 1 1 I n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 18.40 18.60 18.80 1900

00467.D SCAN508.M Mon Jan 14 10:47:06 2002 Page 5

NYC-WTC_000051461

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NYC-WTC_000051461Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · similarity 0.996

machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · similarity 0.995

machine-extracted · confidence unavailable · Check page ↗

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