Laboratory report for sample AD31675 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
NYC-WTC_000050294–000050316Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data. File : C:\MSDCHEM\1\5973N\02JAN24\31675A.D Vial: 2 Acq On : 24 Jan 2002 12:31 pm Operator: Sample : 508scan; re-inj Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 5-Nitro-2-furaldoxime $$ 2-... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 18.85 1.73 ug/L 1121230 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 5-Nitro-2-furaldoxime $$ 2-Furan... 156 C5H4N2O4 000555-15-7 42 0
P 2 Pyrazole, 3-(p-chlorophenyl)-5-m... 192 C10H9C1N2 017629-27-5 9 A9 3 Benzene, l-bromo-4-chloro- 190 C6H4BrCl 000106-39-8 9 C0b 4 Benzene, l-bromo-3-chloro- 190 C6H4BrCl 000108-37-2 9 0 Abundance Scan 1356 (18.855 min): 31675A.D(-) m/z 191.80 100.00% 64 192
5000 128 96 44 .1 76 | ।............... 160................. ‘ 18.60 18.80 19.00 19.20 1 .. ।.... ।. i. > ।.. <. ।. 1’1011119011180010—30900810 11 | i | 1111 i 11! , > , > | i i I i i 11 1 > 11 11 +TTTT m/z 64.00 / 87.31% ^-> 2030405060 70 8090 100 110 120 130 140 150 160 170 180 190 200 Abundance #54546: 5-Nitro-2-furaldoxime $$ 2-Furancarboxaldehyde, 5-... 33 64 54 5000 58 126 138 108 156 18.60 18.80 19.00 19.20 m/z 127.90 / 31.34% 96 -rrrp-rrryrrT 111 ■■ i • ■ ■i'" l*•1> i >• TT"T‘‘ETTTOEAU‘‘71"7 miz—> 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 Abundance #102437: Pyrazole, 3-(p-chloropheny!)-5-methyl- 192
18.60 18.80 19.00 19.20 1 5000 m/z 193.80 / 23.83% 42 128 75 111 .It 151 , 177 || PIPmmTTLTTT IltI>I I I I II I I>I I I I > II I I I I . I r TTITT n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #99524: Benzene, 1-bromo-4-chloro- ‘ ' I ' ‘ 1 1 1 1 1 1 1 I 1 1 1 1 1 1 1 1 1912 18.60 18.80 19.00 19.20 m/z 95.90 14.77% 5000
50 , 75 96 111
1.....‘A4AB8BAt28**AA***A-8AA1*8**/**** 11 । । al > । ■ 11 ■ । > Jl ■ । > > > > । "**I 130............... ............... /4e i •" ■ i “i" n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 18.60 18.80 19.00 19.20
31675A.D SCAN508.M Thu Jan 24 15:25:30 2002 Page 7
NYC-WTC_000050308
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NYC-WTC_000050276
Laboratory report documenting GCMS analysis of sample AD31674 with detection of unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050317
Laboratory report for sample AD31676 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050258
Laboratory report documenting GCMS analysis of sample AD31664 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051024
Laboratory report documenting GCMS blank analysis to verify system cleanliness during January 8-10, 2002 testing.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050205
Laboratory report documenting GCMS analysis of sample AD31647 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050222
Laboratory report documenting GCMS analysis of sample AD31645 with detection of unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050397
Laboratory report for sample AE00698 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050024
Laboratory report showing GCMS analysis of sample AD31671 including unknown compounds and surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050354
Laboratory report for sample AE00100 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050370
Laboratory report for sample AE00101 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018830
GCMS report for sample AD28861 showing detection of unknown compounds and surrogate recovery data.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003981
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
2 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000050177
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050178
Instrument log sheet recording sample counts and operational parameters for GCMS Method 508 analysis in January 2002.
Filed in the same folder
NYC-WTC_000050180
Calibration report for GCMS analysis of sample AD31647 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000050184
Reference scan data for GCMS analysis of sample AD31647 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000050189
Blank analysis report for GCMS testing of sample AD31647 confirming no contamination above detection limits.
Filed in the same folder