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← Document results/DEP Box 28/GCMS X 1/3/02 A 1/22 - 1/23/02
Document / 23 pages

GCMS analysis results for sample AD31675, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AD31675 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050294–000050316

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”

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Scanned page image, NYC-WTC_000050307
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\O2JAN24\31675A.D vial: 2 Acq On : 24 Jan 2002 12:31 pm Operator: Sample : 508scan; re-inj Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 Cyclopentasiloxane, decamet... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T.

12.54 0.22 ug/L 134458 Naphthalene-d8 13.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 59 3 Pentasiloxane, 1,1,3,3,5,5,7,7,9... 356 C10H32O4Si5 000995-83-5 40 4 Benzeneacetic acid, .alpha.,3,4-... 472 C20H4005Si4 037148-65-5 32 Abundance Scan 803 (12.541 min): 31675A. D (-) m/z 73.10 100.00% 73

5000 267 355 / 1........................... 12.20 12.40 12.60 12.80 ' ' ' mfe-> 4 40 60 154 191 251 ’I’U1t0’EETI’I/1’m111111’1’11111110*811033ET"-"I’O’1T’17’1-11111627U3 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 323339 m/z 267.00 45.35% Abundance #313065: Cyclopentasiloxane, decamethyl- 73

5000 267 T T 1 II It 12.20 12.40 12.60 12.80 355 rn/z 355.10 36.73% 45 I । 193 223 323339 । i . j . । । . j i . । . •{ » । । T j । n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 12.20 12.40 12.60 12.80 267 m/z 356.10 12.72% 5000

,_________________ 191207 323339 251■ i' “tTPPTTTTTTTT ■ i ‘ ■ i “ 1 ‘ i ■" ' i “ “ i'1 “ i1 ■111 “ “ i “ “ i1

miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #302654: Pentasiloxane, 1,1,3,3,5,5,7,7,9,9-decamethyl- ■ ■ i ■ ' ■ ■ i ■ ■ 73 267 12.20 12.40 12.60 12.80 m/z 268.00 9.22% 133 5000 341 207 232

’I’T ...... 1.... 2 . ■ | 326 1 356 ' I ' ‘ " I ' " ' ! ‘ ' 11 I ' miz—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 12.20 12.40 12.60 12.80

31675A.D SCAN508.M Thu Jan 24 15:25:29 2002 Page 6

NYC-WTC_000050307

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NYC-WTC_000050307Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · similarity 0.995

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