Laboratory report for sample AD31675 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
NYC-WTC_000050294–000050316Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\O2JAN24\31675A.D vial: 2 Acq On : 24 Jan 2002 12:31 pm Operator: Sample : 508scan; re-inj Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 Cyclopentasiloxane, decamet... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T.
12.54 0.22 ug/L 134458 Naphthalene-d8 13.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 59 3 Pentasiloxane, 1,1,3,3,5,5,7,7,9... 356 C10H32O4Si5 000995-83-5 40 4 Benzeneacetic acid, .alpha.,3,4-... 472 C20H4005Si4 037148-65-5 32 Abundance Scan 803 (12.541 min): 31675A. D (-) m/z 73.10 100.00% 73
5000 267 355 / 1........................... 12.20 12.40 12.60 12.80 ' ' ' mfe-> 4 40 60 154 191 251 ’I’U1t0’EETI’I/1’m111111’1’11111110*811033ET"-"I’O’1T’17’1-11111627U3 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 323339 m/z 267.00 45.35% Abundance #313065: Cyclopentasiloxane, decamethyl- 73
5000 267 T T 1 II It 12.20 12.40 12.60 12.80 355 rn/z 355.10 36.73% 45 I । 193 223 323339 । i . j . । । . j i . । . •{ » । । T j । n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #313068: Cyclopentasiloxane, decamethyl- 73
355 12.20 12.40 12.60 12.80 267 m/z 356.10 12.72% 5000
,_________________ 191207 323339 251■ i' “tTPPTTTTTTTT ■ i ‘ ■ i “ 1 ‘ i ■" ' i “ “ i'1 “ i1 ■111 “ “ i “ “ i1
miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #302654: Pentasiloxane, 1,1,3,3,5,5,7,7,9,9-decamethyl- ■ ■ i ■ ' ■ ■ i ■ ■ 73 267 12.20 12.40 12.60 12.80 m/z 268.00 9.22% 133 5000 341 207 232
’I’T ...... 1.... 2 . ■ | 326 1 356 ' I ' ‘ " I ' " ' ! ‘ ' 11 I ' miz—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 12.20 12.40 12.60 12.80
31675A.D SCAN508.M Thu Jan 24 15:25:29 2002 Page 6
NYC-WTC_000050307
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NYC-WTC_000050276
Laboratory report documenting GCMS analysis of sample AD31674 with detection of unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050317
Laboratory report for sample AD31676 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050258
Laboratory report documenting GCMS analysis of sample AD31664 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051024
Laboratory report documenting GCMS blank analysis to verify system cleanliness during January 8-10, 2002 testing.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050205
Laboratory report documenting GCMS analysis of sample AD31647 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050222
Laboratory report documenting GCMS analysis of sample AD31645 with detection of unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050397
Laboratory report for sample AE00698 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050024
Laboratory report showing GCMS analysis of sample AD31671 including unknown compounds and surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050354
Laboratory report for sample AE00100 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050370
Laboratory report for sample AE00101 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018830
GCMS report for sample AD28861 showing detection of unknown compounds and surrogate recovery data.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003981
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
2 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000050177
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050178
Instrument log sheet recording sample counts and operational parameters for GCMS Method 508 analysis in January 2002.
Filed in the same folder
NYC-WTC_000050180
Calibration report for GCMS analysis of sample AD31647 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000050184
Reference scan data for GCMS analysis of sample AD31647 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000050189
Blank analysis report for GCMS testing of sample AD31647 confirming no contamination above detection limits.
Filed in the same folder