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GCMS analysis results for sample AD31676, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AD31676 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050317–000050333

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02

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Scanned page image, NYC-WTC_000050326
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data .File : C:\MSDCHEM\1\5973N\02JAN23\31676.D Vial: 1 Acq On : 23 Jan 2002 2:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 Benzene, 1-bromo-3-chloro- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 18.74 1.53 ug/L 784065 Ac enaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzene, l-bromo-3-chloro- 190 C6H4BrCl 000108-37-2 9

P 2 Benzene, l-bromo-2-chloro- 190 C6H4BrCl 000694-80-4 9 3 Pyrazole, 3-(p-chlorophenyl)-5-m. .. 192 C10H9C1N2 017629-27-5 9 4 2-Norbornanone, 1~(epithioethyl)... 228 C11H16O3S 001782-93-0 9 Abundance Scan 1346 (18.741 min): 31676.D (-) m/z 191.80 100.00% 64 192

5000 128 96 162 180 18.40 18.60 18.80 19.00 O ' 1 | “ " I '‘ TTJ■ l .>|. ThmPRHn 1111 ■ ‘' i ‘ ■ I" " I' "" l""i Terr m/z 64.00 97.12% miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #99522: Benzene, 1-bromo-3-chloro- 192

75 111 5000 TPIT 50 18.40 1 8.60 18.80 19.00 34.66% m/z 127.90 — O-mmpr | "'r1 Tpm’ , ..t....130 1 1।।। । ■ j > । 96 "i “ miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #99515: Benzene, 1-bromo-2-chloro- 192 111 -A/.... . 5000

miz-> 0 TU

Abundance 35 50 75

i , 154 . ।।।.111>> P।।।>111n111111111111111 ,1111 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #102437: Pyrazole, 3-(p-chloropheny!)-5-methyl- ’ 1’’ Pr 18.40 18.60 18.80 19.00 m/z 193.80 26.77%

P ' ' I ' ‘ ‘ ‘ I ‘ ‘ ' ■ I ' ' ' ‘ I ‘ ‘ ‘ ‘ 1 1 192 18.40 18.60 18.80 19.00 m/z 95.90 17.84% 5000

42 75 128

O-m 111 | . 151,. 177. 11 ' ‘i" T ’ I * ‘ ‘ ’ I • ‘ ‘ • I ' * ‘ ' I ' n/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 18.40 18.60 18.80 19.00

31676.D SCAN508.M Thu Jan 24 09:57:33 2002 Page 6

NYC-WTC_000050326

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NYC-WTC_000050326Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · similarity 0.996

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