GCMS analysis results for sample AE12161, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052302\12161.D Vial: 14 Acq On : 23 May 2002 8:33 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant-Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 8 1-Benzopyrylium, 2-phenyl- Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 5.38 0.29 ug/L 160748 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qua. 1 1-Benzopyrylium, 2-phenyl- 207 C15H110 014051-53-7 5 2 4-Bromo-3-chloroaniline 205 C6H5BrClN 021402-26-6/5 3 Benzenamine, 4-bromo-2-chloro- 205 C6H5BrClN 038762-41-3 5 4 2-Methyl-6-(5-methyl-2-thiazolin... 207 C10H13N3S 1000225-39-3 5 Abundance Scan 391 (5.377 min): 12161.D (-385) (-) m/z 207.00 100.00% 207

5000 96 49 83

n/z-> 0 1.. .j.... 14।j. I..j।।. r-rrr 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 5.00 m/z 208.00 5.20 5.40 5.60 49.52% 5.80

Abundance #84871:1 -Benzopyrylium, 2-phenyl- 207

5000 36 5.00 5.20 5.40 5.60 5.80 I 77 131 178 m/Z 96.00 37.98% 27 , | 51 63 189 102 115 152 165 , 194 . 0: -4-++4***#*--++4-p-*-t- mmm—T n/z-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #84857:4-Bromo-3-chloroaniline 2017 ' l ' ‘ ' I ‘ ' I ■ ' ‘ ‘ I ‘ 5.00 5.20 5.40 5.60 5.80 5000 m/z 49.10 31.979 90 99 126 E 63 n/z-> 0: Tp E,7,— ‘ ' 'I' ' “ I “ mkmpmmmpmgmpm 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 4——m Abundance #84854: Benzenamine, 4-bromo-2-chloro- 2017 5.00 5.20 5.40 5.60 5.80 m/z 44.10 20.31% 90 5000 63 126 44. 99

m/z—> —43.4 0- ' I ‘‘ I' 1,108117 B4—2—d441’4"1* 143153 169179 j.... ] r... ।.... ।. .-j. > i’’l 11 > 111111111 rp 1' r 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 5.00 5.20 5.40 5.60 5.80

12161.D 052202.M Wed May 29 09:54:43 2002 Page 10

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