GCMS blank analysis results, June 5 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\060402\604LB.D Vial: 3 Acq On 4 Jun 2002 5:29 pm Operator: McLean Sample 6/4 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST9 8.L

Peak Number 12 1-Benzopyrylium, 2-phenyl- Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 5.36 0.51 ug/L 252044 1,4-dichlorobenzene-d4 9.90 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1-Benzopyrylium, 2-phenyl- 207 C15H110 014051-53-79 2 Ethanol, 2,2,2-trichloro- 148 C2H3C130 000115-20-8 9 3 N-Cyano-N' ,N' ,N' ' ,N' ' -tetramethy. . . 207 C8H13N7 074150-88-2 7 4 Benzenamine, 4-bromo-2-chloro-______ 205 C6H5BrClN 038762-41-3 5 Abundance Scan 389 (5.365 min): 604LB.D (-385) (-) I m/z 207.00 100.00% 207

5000 49

83 96 500 5.20 5.40 5.60 5.80

n/z-> 0- — 20 31 40 r60 —80l ■ 100 l—. 120 140 160 —180r200 m/z 49.10 49.30% Abundance #84871:1-Benzopyrylium, 2-phenyl- 207

5000 36 500 5.20 5.40 5.60' 5.80 131 178 m/z 208.00 39.63% 26 51 63 7 89 102 115 152 165 , 194 L 0- —m. । 17 . |"lr . i' miz-> 20 40 60 80 100 120 140 160 180 200 Abundance #108333: Ethanol, 2,2,2-trichloro- 31

5.00 5.20 5.40 5.60 5.80 5000 m/z 51.00 22.65%

nz-> 0- -18— 4-61 20 40 49

60 77 , L.. 95 113 1123133 148 ......... 111 1 i ’i" i'll 114 y । i i i । । i ■ i । । । i i । । । । । i । । 80 100 120 140 160 180 200 "“hpozMPL...., Abundance #84777: N-Cyano-N‘,N‘,N",N"-tetramethyl-1 ,3,5-triazinetr... ' * i ■ ' 1 ■ i • i i ' i 1 1 1 1 1 1 1 ' 1 1 1 207 5 00 5.20 5.40 5.60 5.80 m/z 209.10 21.86% 135 5000 192 44 178 164 71 82 ........... 11 II 961...............123 1 152 । , Ji ,, 0 ■ ■ i ■ ■ ' ■ i * ' i * f ’ * i * ‘ • 1 i 1 1 1 1 r1 * , 1 1, n/z-> 20 40 60 80 100 120 140 160 180 200 5.00 5.20 5.40 5.60 5.80

604LB.D 060302.M Wed Jun 05 12:28:49 2002 Page 15

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