Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00465 conducted on January 18, 2002.
NYC-WTC_000051222–000051235Folder label: “GCMS X 1/8/02 A 1/10/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\1\5973N\02JAN10\00328.D Vial: 1 Acq On 10 Jan 2002 2:49 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L
Peak Number 3 Silane, tetramethyl- Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
5.89 4.89 ug/L 1575590 1,4-Dichlorobenzene-d4 9.72
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 38 2 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 33 33-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 4 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 Abundance Scan 220 (5.886 min): 00328.D (-) m/z 73.10 100.00% 70
5000 43 .............. , ................... 87 103 5.60 5.80 6.00 6.20 I I 55 o1TTT -PPPPP +PmPmPPP i ■' ■ ■ i T‘ m/z 43.10 24.08% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4814: Silane, tetramethyl- 73
5000 5.60 5.80 6.00 6.20 45 m/z 45.10 9.19% 15 | 53 1 88 .................................... 0 ■' i" " i1 " ■ i' rri । l Pi , rrh*l"1 ■ > i i । t 1 ” I " ' 11 ' " ' I " 1 ' 1 1 " 1 11 1 "T V m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #9702: Butane, 2-methoxy-2-methyl- $$ Ether, methyl tert-p... 73 5.60 5.80 6.00 6.20 5000 m/ z 41.10 8.99% 55 87 27 45 m/z-> o1 TT__ I ‘Tt1I‘1111 I —0I0‘011713 H i " '' i " " i'' " i1 " 11'' " 1111' I 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... ■ ■ । ‘ ‘ ‘"I 1111 n”'111'1 11 70 5.60 5.80 6.00 6.20 m/ z 71.10 6.09% 5000 43 27 87 m/z-> O' jvmn 11 10 20 TIIr 55 , i P 113 i " ' • i'1 ■' r ■' ■ i'1'1 r 11' i'''' i 174 111' ■ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20
)0328.D SCAN508.M Fri Jan IT 10:08:21 2002 Page 5
NYC-WTC_000051230
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NYC-WTC_000051024
Laboratory report documenting GCMS blank analysis to verify system cleanliness during January 8-10, 2002 testing.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050370
Laboratory report for sample AE00101 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051471
Laboratory report showing GCMS analysis of sample AE00469 with surrogate recovery data on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050222
Laboratory report documenting GCMS analysis of sample AD31645 with detection of unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050334
Laboratory report for sample AD31677 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051380
Laboratory report showing GCMS analysis of sample AE00315 with surrogate recovery data on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051453
Laboratory report showing GCMS analysis of sample AE00467 with surrogate recovery data on January 24, 2002.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050354
Laboratory report for sample AE00100 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050397
Laboratory report for sample AE00698 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051394
Laboratory report showing GCMS analysis of sample AE00321 with surrogate recovery data on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050384
Laboratory report for sample AE00103 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051283
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00473 conducted on January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000051152
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
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NYC-WTC_000051153
Document header page containing identification codes and metadata for GCMS files processed in early January 2002.
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NYC-WTC_000051156
Laboratory report detailing GCMS analysis of sample AE00327 for volatile organic compounds on January 10-11, 2002.
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NYC-WTC_000051165
Laboratory report showing GCMS analysis of reference standards used for calibration during January 10-11, 2002 testing.
Filed in the same folder
NYC-WTC_000051179
Laboratory report documenting GCMS blank analysis to verify system cleanliness during January 10-11, 2002 testing.
Filed in the same folder