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← Document results/DEP Box 28/GCMS X 1/9/02 A 1/29/02
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GCMS blank analysis for sample AE00555, Jan-Feb 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS blank analysis results for sample AE00555 conducted between January 29 and February 1, 2002.

NYC-WTC_000051512–000051530

Folder label: “GCMS X 1/9/02 A 1/29/02

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Scanned page image, NYC-WTC_000051523
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

- Data File : C:\MSDCHEM\1\5973N\02JAN29\0109B.D Vial: 1 Acq On : 29 Jan 2002 10:31 am Operator: Sample : lab blank 1/9 Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.89 3.77 ug/L 1645940 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm • CAS# Qual

1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 37 23-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 3 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 4 Silane, tetramethyl- $$ Tetramet... 88 C4H12Si 000075-76-3 9 Abundance Scan 220 (5.885 min): 0109B.D (-) m/z 73.10 100.00% 73

5000 43 5.60 5.80 6.00 6.20

m/z-> 44155. " I" "I"‘11 mP. 87 103 TI*antm 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 I' •'' I m/z 43.10 23.54% Abundance #4814: Silane, tetramethyl- 73

5000 5.60 5.80 6.00 6.20 m/ z 45.10 9.87% 45 TTTTPTTTTT "'ll, 11"!53 15 88 | 11 i 1111 Vsspssssstsess‘‘I"dus**I‘***‘*‘I‘‘***‘S‘* /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 1 ' I ' ' ' ' I ' ' T-r-I-r-r-r-T- 5.60 5.80 6.00 6.20 5000 m/z 41.10 9.03% 43 27 " 111111' 55 , i ri lTi'i ।' ' r ' “ I " ' 'T' Pp 87 113 174 mfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester • 1 1 1 i' ■ i 1 1 ■ ’ 73 5.60 5.80 6.00 6.20 m/z 71.10 6.70%

L 5000

43

tnlz-> 27 55 TTTTTTTTTT TT .87 113 174 r''' i' " ' r ''' i'''' i 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 i ■ " ■ i TUUTT 5.60 b 5.80 6.00 6.20

0109B.D SCAN508.M Wed Jan 30 09:02:33 2002 Page 9

NYC-WTC_000051523

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NYC-WTC_000051523Source: NYC Law Department, mirrored locally

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