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← Document results/DEP Box 28/GCMS X 1/9/02 A 1/29/02
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GCMS blank analysis for sample AE00555, Jan-Feb 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS blank analysis results for sample AE00555 conducted between January 29 and February 1, 2002.

NYC-WTC_000051512–000051530

Folder label: “GCMS X 1/9/02 A 1/29/02

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Scanned page image, NYC-WTC_000051524
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN29\0109B.D Vial: 1 Acq On : 29 Jan 2002 10:31 am Operator: Sample : lab blank 1/9 Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 8 Cyclopentasiloxane, decamet... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 12.54 0.13 ug/L 81429 Naphthalene-d8 13.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 83 2 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 64 3 3,4-Dihydroxybenzyl alcohol,tris... 356 C16H3203Si3 068595-79-9 42 4 1,1,3,3,5,5,7,7-OCTAMETHYL-TETRA... 282 C8H2603Si4 000000-00-0 33 Abundance Scan 803 (12.542 min): 0109B.D (-) m/ z 73.10 100.00% 73

5000 267 355 . r । pp । pr । । ।

154 193 251 j 12.20 12.40 12.60 12.80 45 i TTTOTTWTPTTWIPWIWIIPTPTDT > ■ । ■ ■ ■ ■ । • ■ • • ।' m/z 267.00 47.71% ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 IT i '' ' ' 1 i 1 12.20 12.40 12.60 12.80 m/z 355.10 35.35% 191207 251 1 323339 T001——0000uu0‘—uon—tu—nnu0au—nnmumuutr TITPTTRTTT m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

12.20 12.40 12.60 12.80 5000 267 m/z 268.00 10.37% 355 45 I— 193 223 251 - 323339 J TETEusmmuumummTmuamor 11 ■ " ' i ’1111'1111 " m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #302823: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- TTB—nmnm I 1 1 1 11 ' 11 ‘ I1 73 12.20 12.40 12.60 12.80 m/z 357.20 9.99% 267 5000 179 356 45 147 209 237 , 312 341 L TIPPPPIPITTPT ■ | ■ ■ ■ • | | ■ ■ ' ■ | • T. . , . . . . | . 1 . . . . ( > . ■ T’T ' 1 । 1 1 । । ■ I ' ' ' • I ' ' ‘ ' I ' /z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 12.20 12.40 12.60 12.80

)109B.D SCAN508.M Wed Jan 30 09:02:33 2002 Page 10

NYC-WTC_000051524

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NYC-WTC_000051524Source: NYC Law Department, mirrored locally

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