DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\5973N\02FEB01\0129B.D Vial: 1 Acq On : 1 Feb 2002 10:35 am Operator: Sample : lab blank 1/29 Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Cyclopentasiloxane, decamet... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

12.54 0.19 ug/L 111804 Naphthalene-d8 13.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5- 000541-02-6 83 2 N-(Trifluoroacetyl)-N,0,0',O''-t... 553 C22H42F3NO4Si4 000000-00-0 43 3 Phenethylamine, N-methyl-.beta., .. . 399 C18H37NO3Si3 010538-85-9 43 4 Cyclopentasiloxane, decamethyl - 370 C10H30Q5Si5 000541-02-6 43 Abundance Scan 803 (12.541 min): 0129B.D (-) m/z 73.05 100.00% 73

5000 267 355 .. ............ . 45 12.20 12.40 12.60 12.80 154 193 , । 01 — m/z 267.00 47.45% Tl/Z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 12.20 12.40 12.60 12.80 m/z 355.10 42.86% 207 ,M**** , i 323 0 1 1 1 ",4 ■ ' । ■ 1 1 । ■ ■ ■ ■ । 1 1 1 ' i 1 1 n/z- > 50 100 150 200 250 300 350 400 450 500 550 Abundance #377151: N-(Trifluoroacetyl)-N,O,O,,O"-tetrakis(trimethyl... 73

355 12.20 12.40 12.60 12.80 5000 m/z 356.10 18.37%

45 - 147 193 267 538 0 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #331718: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethy... ■ ■ i > ■ ■ ■ । ■ ■ । ■ 1 ' ' । 1 ' ■ ■ । ‘ 73 12.20 12.40 12.60 12.80 m/z 268.00 12.48%

5000 355 I 44 ill , . 147 193 267294 1 0 ' 'I ' ' ' ' I ' ■ ■ i ' ■ > 1 i ■ ■ 114**1 ** ‘ ‘ I’ /z—> 50 100 150 200 250 300 350 400 450 500 550 12.20 12.40 12.60 12.80

0129B.D SCAN508.M Mon Feb 04 08:40:59 2002 Page 10

NYC-WTC_000004004