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← Document results/DEP Box 28/GCMS X 1/9/02 A 1/29/02
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GCMS analysis results for sample AE00616, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE00616 conducted on February 1, 2002.

NYC-WTC_000051642–000051659

Folder label: “GCMS X 1/9/02 A 1/29/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN29\00616.D Vial: 5 Acq On : 29 Jan 2002 5:59 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 Cyclopentasiloxane, decamet... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 12.54 0.09 ug/L 67485 Naphthalene-d8 13.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 45 3 Phenethylamine, N-methyl-.beta. ,... 399 C18H37NO3Si3 010538-85-9 37 4 3,4-DIHYDROXYMANDELIC ACID-TETRATMS 472 C20H4005Si4 000000-00-0 37 Abundance Scan 803 (12.541 min): 00616.D (-) m/ z 73.10 100.00% 73

5000 267 355 . n 11 I 1

12.20 12.40 12.60 12.80

/z-> 45 211—— 193 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 m/z 267.00 41.22% Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 TT 12.20 12.40 12.60 12.80 m/z 355.10 39.84% 191207 323339 ■ ■ । ■ i ■. ■ ■ i.. ■ ■ i ■ ■ ■. i TE—r—r T’’ n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #313065: Cyclopentasiloxane, decamethyl- 73 .................... 12.20 12.40 12.60 12.80 5000 267 m/z 356.10 13.27% 355 45 193 223 251 t , | । 1 '' I '' 1' 111111 ’' 1'I''1'11‘1111'111 111' I' '' ' I nPp ■ i' ■ ■323339 11''111''11111 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #331718: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethy... 1 ■ i ■ ' • t i ‘ ■ TT 73 12.20 12.40 12.60 12.80 m/z 268.00 11.98%

5000 355

44

11 ‘II‘ ■ ■ ।1 1,88 —T’TuupuuuouumuuuumuCUTTTTTOTETTTT 130147 193 267 294 ’ - ' i • ■ • ■ i 1 • }*"′ i { r r t i-p m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 12.20 12.40 12.60 12.80

)0616.D SCAN508.M Wed Jan 30 09:02:27 2002 Page 9

NYC-WTC_000051654

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NYC-WTC_000051654Source: NYC Law Department, mirrored locally

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