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GCMS analysis results for sample AE00616, Feb 2002

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Laboratory report showing GCMS analysis results for sample AE00616 conducted on February 1, 2002.

NYC-WTC_000051642–000051659

Folder label: “GCMS X 1/9/02 A 1/29/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN29\00616.D Vial: 5 Acq On : 29 Jan 2002 5:59 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Phenanthrene, 9-methyl- $$ ... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 22.28 0.19 ug/L 178700 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 53 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 53 3 Pyrazine, tetraethyl- (CAS) $$ t... 192 C12H20N2 038325-19-8 50 4 1,4-Dimethyl-3,5-propanobicyclo [... 192 C13H20O 000000-00-0 47 Abundance Scan 1656 (22.280 min): 00616.D (-) m/z 192.10 100.00% 192

5000

— 82 96 m/km 42 52 70 । n—1*TTTTTTIPTTTI 118 T 160 +p 22.00 22.20 22.40 22.60 m/z 191.10 18.72% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192

5000 A I ' ' 22.00 22.20 22.40 22.60 m/z 193.10 15.92% 96 88 J 139 152 165 176 I' ” ' I H " I ' ‘IH1*I p'" I T-T-p-l /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192 n. a 22.00 22.20 22.40 22.60 5000 82 m/z 146.10 15.10%

54 110 30 . 94 160 ■ " ■ I'" ■ i11" i' " i11 ■ ■ i ■ TH 11111917711 TWTTTTTTTTTT ‘‘111 /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103348: Pyrazine, tetraethyl- (CAS) $$ tetraethyl pyrazine 192 . A . 22.00 22.20 22.40 22.60 m/ Z 96.10 15.00% 177 5000 1 1 I'1 1 11 ).

53, 67 81 TTTHTTATLTTTUTLTITTTLWTPTTITTTTITTUTUTIT 149 I63 1 ■ i11 4AL m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

30616.D SCAN508.M Wed Jan 30 09:02:27 2002 Page 10

NYC-WTC_000051655

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NYC-WTC_000051655Source: NYC Law Department, mirrored locally

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NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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