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GCMS analysis report for sample AE01510, March 2002

Machine-extracted title · confidence 100%

GCMS laboratory results for sample AE01510 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

NYC-WTC_000010027–000010046

Folder label: “GCMS X 1/23/02 A 2/21/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB21\01510.D Vial: 5 Acq On : 21 Feb 2002 2:17 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 Phenanthrene, 9-methyl- $$ ... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

22.28 0.13 ug/L 98114 Phenanthrene-dlO 22.64

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 53 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 52 3 Pyrazine, tetraethyl- (CAS) $$ t... 192 C12H20N2 038325-19-8 47 4 lH-2-Indenone,2,4,5,6,7,7a-hexah... 192 C13H20O 000000-00-0 40 Abundance Scan 1675 (22.283 min): 01510.D (-) m/z 192.00 100.00% 1912

5000

96 146 160 k 22.00 22.20 22.40 22.60 0 mpmmpmmppm 70 82 1118...... ।... b,.,.-.- m/z 95.90 19.97% mfe-> 2030405060 70 8090 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl-$$ 9-Methylphenanthrene 1512

5000 22.00 22.20 22.40 22.60 m/z 191.00 16.73% 96

miz—> 0 88 , 139 152 165 176 -HPH ""i ■ “■ i■■ ■ • i■'■ ■ i"■ ■ i■ ■ ■ ‘i1 ■ ■11■''11"■'i■ ■ “i“‘■ i■ '’i""i1"■ i ′—

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 U Abundance #88409: N-perdeuteriobenzylideneaniline 1912

22.00 22.20 22.40 22.60 5000 82 m/z 146.10 15.10% 54 110 30 . 94 160 niz—> 0 phgi.... TTTTpTTTJTTTrp-rrrp- iragasgac I » I I I • i"1111 T’ITTTTFTT 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103348: Pyrazine, tetraethyl- (CAS) $$ tetraethyl pyrazine 1912 22.00 22.20 22.40 22.60 m/z 193.00 14.70% 177 5000

81 53 67 mH 0 — 1’1100101111113317111121111171111811117 1193.01. I... 11 149 rrrrp- ,1 mfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

01510.D HP022102.M Mon Feb 25 10:55:10 2002 Page 12

NYC-WTC_000010042

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NYC-WTC_000010042Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.998

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