GCMS analysis results for sample AD31671, Jan 28 2002

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Laboratory report showing GCMS analysis of sample AD31671 including unknown compounds and surrogate recovery data.

NYC-WTC_000050024–000050038

Folder label: “GCMS X 1/3/02 A 1/17/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C: \MSDCHEM\1\5973N\02JAN17\31671.D Vial: 6 Acq On : 17 Jan 2002 6:59 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 Cyclopentasiloxane, decamet... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T.

12.54 0.12 ug/L 55147 Naphthalene-d8 13.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 40 3 N-Methyladrenaline, tri-TMS 413 C19H39NO3S13 000000-00-0 23 4 Benzeneacetic acid, .alpha.,3,4-... 472 C20H4005Si4 037148-65-5 23 Abundance Scan 803 (12.541 min): 31671.D (-) m/z 73.10 100.00% 73

5000 267 355 1 1 12.20 12.40 12.60 12.80 0 45 251 . ........ 4— • ■ i ■ ■.11. m/z 267.00 45.83% mfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 1 ‘ i ■ ■ ■ ■ i ■ • 1 1 1 ' ' ' I ' 1 ' ' 1 1 12.20 12.40 12.60 12.80 m/z 355.10 32.99%

niz-> O' 3X mt 191207 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 " 1 *' 323339 1'1

Abundance #313065: Cyclopentasiloxane, decamethyl- 73 ■ ‘ i ■ ■ ■ ■ i ■ ' ■ । ■ ■ ■ ■ । ■' ■ ■ ।1 12.20 12.40 12.60 12.80 5000 267 m/z 356.00 14.48% 355 45 I . >1.. 0 . i ((i 193।.223 i . i ।.... ।.... ।.... ।.... ।....,.. 221 J f... .'i. .'T. । >r. 323339 । ' l11 'T' n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #339188: N-Methyladrenaline, tri-TMS ■ ■ i * ■ ■ ■ i ‘ ■ ■ । ‘ ■ i ■ • ■ ■ ।1 58 73 12.20 12.40 12.60 12.80 m/z 268.00 11.12%

5000 355

207 It 0 ' ' I ' ‘ ‘ ' I ' ' fl . . । । । । । ।.I । । 27282 308323 Iraaftir । i . i . f. ... । . l'. . |T. . miz—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 12.20 12.40 12.60 1280

31671.D SCAN508.M Tue Jan 22 08:37:27 2002 Page 8

NYC-WTC_000050035

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NYC-WTC_000050035Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AD31585, Jan 28 2002 · Box DEP Box 28

NYC-WTC_000049902

Laboratory report showing GCMS analysis of sample AD31585 including unknown compounds and surrogate recovery data.

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