GCMS analysis results for sample AD31675, Jan 2002

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Laboratory report for sample AD31675 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050294–000050316

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02JAN24\31675A.D Vial: 2 Acq On : 24 Jan 2002 12:31 pm Operator: Sample : 508scan; re-inj Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.17 ug/L 117825 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 64 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 59 3 Benzo[1,2-c:3,4-c]bis(isothiazol ... 192 C8H4N2S2 074960-05-7 45 4 Thiocyanic acid, 2-benzothiazoly ... 192 C8H4N2S2 006011-99-0 45 Abundance Scan 1656 (22.280 min): 31675A.D (-) m/z 192.10 100.00% 1912

5000

92 96 146 160 22.00 22.20 22.40 22.60 54 70 y mmupepnpttrfrt 118111128 j 11 H | rM i rrprmf | >. >> 1111 > 11 .'111 m/z 191.10 15.21% "l..... . ...r n/z—> 2030405060 70 8090 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424: 3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192

5000 ‘22.00 22.20 22.40 22.60 96 164 m/z 96.05 14.71% 1 138 ..!....।.i.,।■।...,। ....।....। ,. I p. . 11 .... । . . . . !. I........... IL i i ■■ ■i ■■ m/z-> 20 30 40 50a) 70 8090 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 1912

22.00 22.-20 22.40 22.60 5000 82 m/z 193.10 14.13%

54 110

m/z—> 30 Tp ' ‘ I | TpHp 94 2030405060 70 8090 100 110 120 130 140 150 160 170 180 W 2(X) 160 ....|....p,-i i j» ri < । > 1111 > m (> 111 j i > 11’ II. Abundance #102104: Benzo(1,2-c:3,4-c]bis(isothiazole) $$ Benzo[1,2-c... 192 AL 22.00 22.20 22.40 22.60 ■ i ■ ■ ■ 1 i

m/z 146.10 13.27% 5000 45 148 57 69 82 96 121 165

miz—> — । > i > 11 > i i । । > i i 11 ( > (। । i i । . 11 . >. । i > j q । (। ′′ n p > i 111 । । । j i

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 mmmm ................. A • 1 t ' * * • i • 1 • * i * 22.00 22.20 22.40 22.60 —r

31675A.D SCAN508.M Thu Jan 24 15:25:30 2002 Page 10

NYC-WTC_000050311

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GCMS analysis results for sample AD31674, Jan 25 2002 · Box DEP Box 28

NYC-WTC_000050276

Laboratory report documenting GCMS analysis of sample AD31674 with detection of unknown compounds and surrogate recovery.

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