GCMS analysis results for sample AD31675, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AD31675 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050294–000050316

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN24\31675A.D Vial: 2 Acq On : 24 Jan 2002 12:31 pm Operator: Sample : 508scan; re-inj Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 2-Norbornanone, 1-(epithioe... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 22.85 3.73 ug/L 2594030 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Norbornanone, 1-(epithioethyl)... 228 C11H1603S 001782-93-0 28 2 (1R*,4R*,5S*)-1-CARBETHOXY-4-MET... 234 C15H2202 043219-76-7 9 3 Cyclohexane-dl2 96 C6D12 001735-17-7 7 4 1,2,5,6-tetrathia-3,7-dimethyl-c... 212 C6H12S4 116664-31-4 7 Abundance Scan 1706 (22.851 min): 31675A.D (-) m/z 64.00 100.00% 64 160

5000 96 224

128 22.60 22.80 23.00 23.20

miz-> 20 43 ■ ■ i '■ ' • • i 40 60 47980— 100 4. 120 1 140 160 180 200 220 240 260 256 ■ ■ i ■ ■ ■ u ' m/z 159.90 83.51% Abundance #156398:2-Norbornanone, 1-(epithioethy!)-7,7-dimethyl-, S... 64 93 120

5000 107 j j I’IT i1 j" j 1 r । 1 j'! * । T1 Pr= 53 79 164 22.60 22.80 23.00 23.20 151 m/z 95.90 45.10%

m/z-> 20 Abundance

5000 34 1 ' I ‘ 1 ■ i 40 60 ' • i ■ • ' ■ i ■ • ■ i 1 ■ ■ ■ i

21 105 1 ■ ■ i • ■ ■ 1 i ■ ■ ■ ' i ■ • • ■ i ■ ■ ■ ■ i 1

80 100 120 140 160 180 200 220 240 260 #165203: (1R*,4R*,5S*)-1-CARBETHOXY-4-METHYL-8-METHYLENE-S...

91 160 119

188 A_ T i ■ ■ ■ • i ■ ■

22.60 22.80 23.00 23.20 m/z 223.80 39.23%

234

• • i ■ ■ ■ ■ i ■ ' ■ ■ i ■ ■ ■ ■ i • ■ ■ ■ j ■ ■ ■ ■ i '1 ' ■ ■ 14 I 1 ■ ■ i ■ ■ ■ • i ■ • ■ ■ i • ■ ■ ■ i ■ niz-> 20 40 60 80 1(X) 120 140 160 180 200 220 240 260 Abundance #3553: Cyclohexane-d12 r"M .‘J . T . < p , I I | I I 1 1 | I I ! 46 64 22.60 22.80 23.00 23.20 m/z 161.90 17.51%

A 96 5000 30 78 . ... 1 ■

m/z—> 20 40 4 60 • > i • > 80 100 i ■ • ■ ■ i • • • 1 i 1 ' 1 1 1 1 1 1 1 1 1 1 ' 1 1 11 ' 1 I ' 1 1 1 1 1 1 ' 1 1 1 120 140 160 180 200 220 240 260 22.60 22.80 23.00 23.20

31675A.D SCAN508.M Thu Jan 24 15:25:30 2002 Page 11

NYC-WTC_000050312

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GCMS analysis results for sample AD31674, Jan 25 2002 · Box DEP Box 28

NYC-WTC_000050276

Laboratory report documenting GCMS analysis of sample AD31674 with detection of unknown compounds and surrogate recovery.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996