Laboratory report for sample AD31676 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
NYC-WTC_000050317–000050333Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN23\31676.D Vial: 1 Acq On : 23 Jan 2002 2:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1 ...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 2-Norbornanone, 1-(epithioe... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 23.46 0.30 ug/L 167872 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Norbornanone, 1-(epithioethyl)... 228 C11H1603S 001782-93-0 36 2 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 9 3 N- (2-Hydroxyethyl) -N’ - [2' - (-meth. . . 255 C10H13N3O3S 000000-00-0 9 4 5-Nitro-2-furaldoxime $$ 2-Furan... 156 C5H4N2O4 000555-15-7 7 Abundance Scan 1759 (23,456 min): 31676.D (-) m/z 64.00 100.00% 64
160 5000 96 224 128 T T T 44 192 , 256 23,20 23.40 23.60 23.80
miz-> Of 40 60 80 rTr 1 I 100 120 140 160 180 200 220I 240 -lL m/z 159.85 56.41% 260 Abundance #156398:2-Norbornanone, 1-(epithicethy!)-7,7-dimethyl-, S... 64 120 93
5000 107 53 164 23.20 23.40 23.60 23.80 79 151 V 95.90 29.11% 34 01 • ■ i ■ 11 i ‘ I* ■ 1 i ■ ■ ■ i ' ■ ■ ■ i ■ ■ i ■ 1 ■ • i 1 1 1 1 i ■ ■ ■ ' i ■ ■ ■ ■ i ■ niz-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #195809: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... 64 ■ ‘ i ■ ' ■ ■ i T T 23.20 23.40 23.60 23.80 5000 m/z 223.80 23.69% 192 128 160 96 48 180....... | 224 256 01 TTPTmt ' 1 1 1 1 1 1 ' 1 ' 1 1 1 I ' 1 1 t ■ ■ ———BBmPIOgm miz—> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #193372: N-(2-Hydroxyethyl)-N’[2’-(-methoxycarbony!)thiop... 64 256 23.20 23.40 23.60 23.80 m/z 161.90 18.31% 128 160 5000 96 192 221
0 1 ■ i ■ ‘ ' ■ i -n-p-r I ■ • ■ ■ i ■ ' I ' 1 1 ‘ I■ ' 1 ' I ' 1 I" nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 23.20 23.40 23.60 23.80
31676.D SCAN508.M Thu Jan 24 09:57:34 2002 Page 10
NYC-WTC_000050330
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NYC-WTC_000050276
Laboratory report documenting GCMS analysis of sample AD31674 with detection of unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050354
Laboratory report for sample AE00100 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050258
Laboratory report documenting GCMS analysis of sample AD31664 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051283
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00473 conducted on January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050370
Laboratory report for sample AE00101 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050205
Laboratory report documenting GCMS analysis of sample AD31647 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051453
Laboratory report showing GCMS analysis of sample AE00467 with surrogate recovery data on January 24, 2002.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050334
Laboratory report for sample AD31677 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050024
Laboratory report showing GCMS analysis of sample AD31671 including unknown compounds and surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050222
Laboratory report documenting GCMS analysis of sample AD31645 with detection of unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018830
GCMS report for sample AD28861 showing detection of unknown compounds and surrogate recovery data.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003981
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
2 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000050177
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050178
Instrument log sheet recording sample counts and operational parameters for GCMS Method 508 analysis in January 2002.
Filed in the same folder
NYC-WTC_000050180
Calibration report for GCMS analysis of sample AD31647 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000050184
Reference scan data for GCMS analysis of sample AD31647 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000050189
Blank analysis report for GCMS testing of sample AD31647 confirming no contamination above detection limits.
Filed in the same folder