Laboratory report documenting GCMS analysis of sample AD31674 with detection of unknown compounds and surrogate recovery.
NYC-WTC_000050276–000050293Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN22\31674.D Vial: 2 Acq On : 22 Jan 2002 3:30 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 2-Norbornanone, 1-(epithioe... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 22.85 4.92 ug/L 3352480 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Norbornanone, 1-(epithioethyl) .. . 228 C11H1603S 001782-93-0 28 80 2 (1R*,4R*,5S*)-1-CARBETHOXY-4-MET... 234 C15H2202 043219-76-7 9 Gvo 3 N- (2-Hydroxyethyl) -N’ - [2' - (-meth. . . 255 C10H13N3O3S 000000-00-0 9 MAT** 4 Cyclohexane-dl2 96 C6D12 001735-17-7 7 Abundance Scan 1706 (22.851 min): 31674.D (-) m/z 64.00 100.00% 64 160
5000- 96 224 111’11* 1 r T 128 - 192 22.60 22.80 23.00 23.20 • ■ । 44 | 76 > i l11 1*1** 1 ■ ■ i ■ ■ 25611 ■ • m/z 159.90 81.09% niz-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #156398:2-Norbornanone, 1-(epithicethy!)-7,7-dimethyl-, S... 64 120 93
5000 107 53 79 164 “ 22.60 22.80 23.00 23.20 ' 151 m/z 95.9.0 42.94% 34 ■ ■ i ■ 1 1 i ‘ I 4* ■ • i 1 r1 1 ri ' l niz-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #165203: (1R*,4R*,5S*)-1-CARBETHOXY-4-METHYL-8-METHYLENE-S... 160 91 119 91 105 22.60 22.80 23.00 23.20 ' 5000 m/z 223.80 40.91% 188 234
1 1 i ‘ 488*185* । । i : : j i niz-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #193372: N-(2-Hydroxyethyl)-N‘-[2‘-(-methoxycarbony!)thiop... fftfmTTr 64 22.60 22.80 23.00 23.20 256 m/z 161.90 17.04% 8000
6000 128 160 4000 96 I . 192 ■ ■ i ■ 1 ■ ■ i ■ ■ i • • ■ । l 1 1 ' 1 I 1 * 1 i * > . | ■ 221 v —A m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 22.60 22.80 23.00 23.20
31674.D SCAN508.M Thu Jan 24 14:00:12 2002 Page 9
NYC-WTC_000050288
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NYC-WTC_000050317
Laboratory report for sample AD31676 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050354
Laboratory report for sample AE00100 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050258
Laboratory report documenting GCMS analysis of sample AD31664 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051453
Laboratory report showing GCMS analysis of sample AE00467 with surrogate recovery data on January 24, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050205
Laboratory report documenting GCMS analysis of sample AD31647 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050222
Laboratory report documenting GCMS analysis of sample AD31645 with detection of unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051283
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00473 conducted on January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050240
Laboratory report documenting GCMS analysis of sample AD31646 with detection of unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018830
GCMS report for sample AD28861 showing detection of unknown compounds and surrogate recovery data.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003981
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011007
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02721 including surrogate recovery.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036779
GCMS analysis report for sample AD29522 listing unknown compounds and surrogate recovery data from February 8, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000050177
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050178
Instrument log sheet recording sample counts and operational parameters for GCMS Method 508 analysis in January 2002.
Filed in the same folder
NYC-WTC_000050180
Calibration report for GCMS analysis of sample AD31647 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000050184
Reference scan data for GCMS analysis of sample AD31647 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000050189
Blank analysis report for GCMS testing of sample AD31647 confirming no contamination above detection limits.
Filed in the same folder