Laboratory report for sample AD31675 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
NYC-WTC_000050294–000050316Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data- File : C:\MSDCHEM\l\5973N\02JAN24\31675A.D Vial: 2 Acq On : 24 Jan 2002 12:31 pm Operator: Sample : 508scan; re-inj Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 2-Norbornanone, 1-(epithioe... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.
23.43 0.25 ug/L 176620 Phenanthrene- dl 0 22.65
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Norbornanone, 1-(epithioethyl) .. . 228 C11H1603S 001782-93-0 36 2 Methyl 5-Amino-2-chloro-4-thiazo... 192 C5H5C1N2O2S 000000-00-0 9 3 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 9 4 N-(2-Hydroxyethyl)-N* -[2f-(-meth... 255 C10H13N3O3S 000000-00-0 9 Abundance Scan 1757 (23.433 min): 31675A.D (-) m/z 64.00 100.00% 64
160 5000 96 192 224 128 . 23.00 23.20 23.40 23.60 23.80 ' 43 BAi) 76 - -tpl, ■ • i ‘ 1 i * i • • • • 11 i 256 )“ ‘ 1 I ■ m/z 159.90 61.75% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #156398:2-Norbornanone, 1-(epithicethy)-7,7-dimethyl-, S... 61 93 120
5000 107 53 79 164 23.00 23.20 23.40 23.60 23.80 ' 151 m/z 95.90 30.55% 34 ■ ' i ■ ■ ' i i 1 1 1 ■ i • • • i ' 1 ‘ • i ' ‘ i 1 ■ ■ ■ i ' ■ • ' i 1 ' • ■ i ■ ■ ■ ' i • nfe-> 40 60 80 100 120 140 160 180 200 220 240 250 Abundance #101902: Methyl 5-Amino-2-chloro-4-thiazolecarboxylate $$... 160
192 23.00 23.20 23.40 23.60 23.80 ' 5000 m/z 223.80 19.34%
79 132 a •’> | i r । । | । । T-r-p-r 1 i 1 ' 1 ' i ‘ > i ■ * ■ ■ i 1 niz-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #195809: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... 64 23.00 23.20 23.40 23.60 23.80 ' m/z 191.80 18.04% 5000, 192 96 128 160 48 | 224 256 /z—> • • t *1 ‘ • i 40 60 mI 80 ------------------------------- ■ ■ i 1 ' 80 100 120 140 160 180 200 220 240 260 T ■j-r-r-n-p-r 23.00 23.20 23.40 23.60 23.80
31675A.D SCAN508.M Thu Jan 24 15:25:30 2002 Page 12
NYC-WTC_000050313
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NYC-WTC_000050276
Laboratory report documenting GCMS analysis of sample AD31674 with detection of unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050317
Laboratory report for sample AD31676 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050258
Laboratory report documenting GCMS analysis of sample AD31664 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051024
Laboratory report documenting GCMS blank analysis to verify system cleanliness during January 8-10, 2002 testing.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050205
Laboratory report documenting GCMS analysis of sample AD31647 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050222
Laboratory report documenting GCMS analysis of sample AD31645 with detection of unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050397
Laboratory report for sample AE00698 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050024
Laboratory report showing GCMS analysis of sample AD31671 including unknown compounds and surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050354
Laboratory report for sample AE00100 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050370
Laboratory report for sample AE00101 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018830
GCMS report for sample AD28861 showing detection of unknown compounds and surrogate recovery data.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003981
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
2 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000050177
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050178
Instrument log sheet recording sample counts and operational parameters for GCMS Method 508 analysis in January 2002.
Filed in the same folder
NYC-WTC_000050180
Calibration report for GCMS analysis of sample AD31647 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000050184
Reference scan data for GCMS analysis of sample AD31647 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000050189
Blank analysis report for GCMS testing of sample AD31647 confirming no contamination above detection limits.
Filed in the same folder