Laboratory report for sample AD31675 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
NYC-WTC_000050294–000050316Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN24\31675A.D Vial: 2 Acq On : 24 Jan 2002 12:31 pm Operator: Sample : 508scan; re-inj Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 3-Methylchromone $$ 4H-1-Be... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 23.70 0.22 ug/L 149615 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual j0 1 3-Methylchromone $$ 4H-1-Benzopy... 160 C1OH802 000085-90-5 50 C 2 4-methyl-5-azacinnoline 160 C8H8N4 000000-00-0 7 3 ACETONE-D6 $$ PERDEUTERO ACETONE... 64 C3D60 000666-52-4 7 4 Benzonitrile, 4-[(methoxyimino)m... 160 C9H8N20 033499-34-2 7 Abundance Scan 1780 (23.696 min): 31675AD (-) m/z 64.00 100.00%
5000 64 160 /W, 96 224
84 , 128 149 192 23.40 23.60 23.80 24.00 — ------- ■ • • ‘ i ■ ■ ‘ • i 1. ■ m/z 159.90 93.76% miz—> 20 40 60 80 100 120 140 160 180 200 220 Abundance #59933:3-Methylchromone $$ 4H-1-Benzopyran-4-one, 3-methy...
64 92
131 160 /aw 1 * 1 | n i i । i n j j 1 i i i1 J1 j 'j" j T"1 5000 77 23.40 23.60 23.80 24.00 104 120 m/z 223.80 36.15%
m/z—> 20 Abundance t"1' >■■■■].. EUT 40 60 *14* 80 100 120 140 • । 160 ■
#59519:4-methyl-5-azacinnoline 160 180 200 220 W‘ 23.40 23.60 23.80 24.00 5000 m/z 95.90 34.95%
miz-> 20 Abundance 103 91 , II 131 --------- ■ I ■ ■ ‘ ■ i 1 ' 1 ■ i ■ ‘ ■ ■ i 1 ■ 40 60 80 100 120 140 160 180 200 220 /WW #591: ACETONE-D6 $$ PERDEUTERO ACETONE $$ 2-PROPANONE-1,1 45 64 23.40 23.60 23.80 24.00 m/z 225.80 23.14%
5000
30 .1 ■ 144th" ■ ■ i 1 **I**1****I*****1****** ■ ■ । ‘ ■r f1 ■1 ' r1 1 1' “ *
iz—> 20 40 60 80 100 120 140 160 180 200 220 23.40 23.60 23.80 24.00
31675A.D SCAN508.M Thu Jan 24 15:25:31 2002 Page 13
NYC-WTC_000050314
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NYC-WTC_000050276
Laboratory report documenting GCMS analysis of sample AD31674 with detection of unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050317
Laboratory report for sample AD31676 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050258
Laboratory report documenting GCMS analysis of sample AD31664 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051024
Laboratory report documenting GCMS blank analysis to verify system cleanliness during January 8-10, 2002 testing.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050205
Laboratory report documenting GCMS analysis of sample AD31647 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050222
Laboratory report documenting GCMS analysis of sample AD31645 with detection of unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050397
Laboratory report for sample AE00698 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050024
Laboratory report showing GCMS analysis of sample AD31671 including unknown compounds and surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050354
Laboratory report for sample AE00100 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050370
Laboratory report for sample AE00101 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018830
GCMS report for sample AD28861 showing detection of unknown compounds and surrogate recovery data.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003981
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
2 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000050177
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050178
Instrument log sheet recording sample counts and operational parameters for GCMS Method 508 analysis in January 2002.
Filed in the same folder
NYC-WTC_000050180
Calibration report for GCMS analysis of sample AD31647 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000050184
Reference scan data for GCMS analysis of sample AD31647 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000050189
Blank analysis report for GCMS testing of sample AD31647 confirming no contamination above detection limits.
Filed in the same folder