GCMS analysis results for sample AD31675, Jan 2002

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Laboratory report for sample AD31675 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050294–000050316

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN24\31675A.D Vial: 2 Acq On : 24 Jan 2002 12:31 pm Operator: Sample : 508scan; re-inj Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1.. .\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 Sulfur, mol. (S8) (CAS) $$ ... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

26.14 78.57 ug/L 54671100 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 96 2 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 95 3 Cyclic octaatomic sulfur 256 S8 010544-50-0 91 4 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 90 Abundance Scan 1994 (26.139 min): 31675A.D (-) m/z 64.00 100.00%) 64

5000 128 256 160 ■ ■ I ‘ ‘ ‘ I ■ ' ‘ 1. I .. I I ... I I 96 192 25.80 26.00 26.20 26.40

niz-> 0- —44 40 —60 1, 7680 100 120 9140 —— 1 180' r‘ • ‘ i • * 160 224 11 j 1 ■ * * i • 200 220 240 260 ‘ t • ■ • • i 1 ■ ‘ • i 1 ■ m/z 127.90 45.75 Abundance #195806: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ 8... 64 256

128 160 5000 . —7, 25.80 26.00 26.20 26.40 96 192 m/z 255.80 43.84 224 34 niz-> TIBnnn 40 60 80 ■ • I 1 1 i • ■ ■ ■ i ■ 100 120 140 160 180 200 220 240 T-r-p-r LH 260 Abundance #195807: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$S8$$ S... 64 25.80 26.00 26.20 26.40 1 5000 m/z 159.90 33.50% 128 256 96 160 192 34 48 ■ ■ ■ ■ i ■ ■ ■ ■ i Il... ■ ■ • i ■ ‘ 1111/11/8 1 1 224 ’ 144441*4**1** z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #195804: Cyclic octaatomic sulfur — T5I• ____ ___________ ’IIT4*PA**1*+*3I4 64 25.80 26.00 26.20 26.40 m/z 95.90 21.65

5000

128 160 192 256

-nfe-> 34 11 I ■ ■ ■ ■ i 40 60 80 100 120 140 160 180 200 220 224 240 H 260 •114* 1** * ‘i • ■ ■ ■ l 1 ■ ■ ■ i ■ 25.80 26.00 26.20 26.40

31675A.D SCAN508.M Thu Jan 24 15:25:31 2002 Page 14

NYC-WTC_000050315

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NYC-WTC_000050315Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AD31674, Jan 25 2002 · Box DEP Box 28

NYC-WTC_000050276

Laboratory report documenting GCMS analysis of sample AD31674 with detection of unknown compounds and surrogate recovery.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996