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GCMS analysis results for sample AD31675, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AD31675 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050294–000050316

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02

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NYC 9/11 Public Portal Document Tentatively Identified Compound (LSC) summary Operator ID: Date Acquired: 24 Jan 2002 12:31 pm Data File: C:\MSDCHEM\l\5973N\02JAN24\31675A.D Name: 508scan; re-inj Mise: January 24, 2002 Method: C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title: 508 scan method Library Searched: C:\DATABASE\WILEY7N.L

--Internal Standard-- TIC Top Hit name RT EstConc Units Response # RT Resp Cone Butanoic acid, me.. 3.61 0.2 ug/L 67677 1 9.72 8362920 20.0 Methacrylamide $$.. 4.25 0.1 ug/L 59657 1 9.72 8362920 20.0 Cyclotetrasiloxan. . 9.41 0.3 ug/L 124919 1 9.72 8362920 20.0 Cyclopentasi loxan. . 12.54 0.2 ug/L 134458 2 13.19 11972900 20.0 5-Nitro-2 raldo.. 18.85 1.7 ug/L 1121230 3 18.34 12997100 20.0 Benzoic a d, 2,5.. 20.93 0.1 ug/L 84607 4 22.65 13917000 20.0 5-Nitro-2 uraldo. . 21.62 0.1 ug/L 68310 4 22.65 13917000 20.0 3-Cyanocarbazole . . . 22.28 0.2 ug/L 117825 4 22.65 13917000 20.0 2 -Norbornanone, 1. . . 22.85 3.7 ug/L 2594030 4 22.65 13917000 20.0 2 -Norbornanone , 1. . . 23.43 0.3 ug/L 176620 4 22.65 13917000 20.0 3-Methylchromone . . . 23.70 0.2 ug/L 149615 4 22.65 13917000 20.0 Sulfur, mol. (88) . . . 26.14 78.6 ug/L 54671100 4 22.65 13917000 20.0

31675A.D SCAN508.M Thu Jan 24 15:25:31 2002 Page 15

NYC-WTC_000050316

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NYC-WTC_000050316Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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