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GCMS analysis results for sample AD31676, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AD31676 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050317–000050333

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02

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Scanned page image, NYC-WTC_000050332
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN23\31676.D Vial: 1 Acq On : 23 Jan 2002 2:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1. ..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 Sulfur, mol. (S8) (CAS) $$ ... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

26.15 89.05 ug/L 50149500 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 96 2 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 94 3 Sulfur $$ Sulfur, precipitated $... 256 S8 007704-34-9 87 4 Cyclic octaatomic sulfur 256 S8 010544-50-0 87 Abundance Scan 1995 (26.150 min): 31676.D (-) m/z 64.00 100.00% 64

5000 128 256 160 96 192 25.80 26.00 26.20 26.40 “ 1 ‘ m/z-> 0- 44 ' ' i 1 • ■ ■ i 40 60 80 476— 100 120 i ■ ■ ■ ‘ i 1 , ... 1 —Pp140— 160 227 180 200 220 240 260 4 m/z 127.90 46.68% Abundance #195806: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... 64 256 160 128 5000 ■ ■ i 1 ■ ■ ■ i ■ ■ ■ ■ I • ■ ■ ■ i ■ ■ ■ ■ i ■ 25.80 26.00 26.20 26.40 96 192 m/z 255.80 45.91% 224 34 1 - niz-> 0- * 11 TT-p-r 40 60 80 ■ ■ i ■ ■ 100 120 140 160 180 200 220 240 1,..... I'. ' 2867 Abundance #195807: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... 64 25.80 26.00 26.20 26.40 ‘ ‘ ‘ 5000 m/z 159.90 33.06% 128 256 96 160 192 48 Or 34 1 1 ' 11** * ■ j ■ ■ i ■ ■ ' 1 i 1 j_____ • • i • • j____________ * | > • • • i > i 224 — ■ i ■ ■ ■ ■ i 1 ■ ■ ■ i ■ miz-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #195801: Sulfur $$ Sulfur, precipitated $$ S $$ Brimstone... 64 192 25.80 26.00 26.20 26.40 “ ‘ ' 128 m/z 95.90 21.75% 160 256 5000 96 224 OPPPT - i ■ ■ ‘ ■ i • .... • ■ ■ ■ ‘ i ■ ■ 1 i ' • • • i ' " ’246' TT r' l ' 1 1 1 i 1 ‘ 1 'T' 1 1 1 I 1 1 1 1 I'1 n/z-> 40 60 80 100 120 140 160 180 200 220 260 25.80 26.00 26.20 26.40

31676.D SCAN508.M Thu Jan 24 09:57:34 2002 Page 12

NYC-WTC_000050332

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NYC-WTC_000050332Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · similarity 0.996

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