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GCMS results for sample AE00467, Jan 24 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00467 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051453–000051470

Folder label: “GCMS X 1/8/02 A 1/11/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C : \MSDCHEM\1\5973N\O2 JAN11\00467 . D Vial: 7 Acq On : 11 Jan 2002 7:05 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 6 3-Methylchromone $$ 4H-1-Be... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

23.42 0.18 ug/L 112228 Phenanthrene-dl0 22.65

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Methylchromone $$ 4H-1-Benzopy ... 160 C10H8O2 000085-90-5 50 O 2 Valine, 3-[sulfothio]- 229 C5H11NO5S2 000000-00-0 40 G0vv 3 cis-endo-3-(2-Isopropoxycarbonyl... 226 C12H1804 000000-00-0 38 ysCov 4 l-Azafluorene $$ 9H-Indeno[2,1-b... 167 C12H9N 000244-44-0 35 Abundance Scan 1756 (23.422 min): 00467.D (-) m/z 64.00 100.00% 64 167

5000

84 96 128 139 224 VAA m/z-> 0 l 1 ■ ■ ' 1 40 60 LX 80 100 120 140 , . ■ pr 160 180 200 220 194 L 256

240 260 23.00 23.20 23.40 23.60 23.80 m/z 167.10 90.11% Abundance #59933: 3-Methylchromone $$ 4H-1-Benzopyran-4-one, 3-methy... 92 160 64 131 5000 77 I 1 ■ ■ ■ i ' ' 1 i ' ■ 104 120 23 00 23.20 23.40 23.60 23.80 m/z 159.85 65.91%

0...60 m/z-> Abundance 40 64 80

75 100 120 140 160 180 #157749: Valine, 3-[sulfothio]- 200 220 240 260

GA 23.00 23.20 23.40 23.60 23.80 5000 48 m/ z 223.80 38.80% 160 96 114 128 194 - 1——80 100 120 140 160 .180 1l,212, n/z-> 0T Abundance 40 60 200 220 #153775: cis-endo-3-(2-lsopropoxycarbonyl)bicyclo[2.2.1)he... 1^7 240 260 yAAAM 23 00 23.20 23.40 23.60 23.80 m/z 95.90 34.86%

5000

UN 118 100 138 227 66 148 I III . 209 I 0T T m/z~> 40 60 80 100 120 140 160 180 200 220 240 260 23.00 23.20 23.40 23.60 23.80

00467.D SCAN508.M Mon Jan 14 10:47:07 2002 Page 8

NYC-WTC_000051464

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NYC-WTC_000051464Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · similarity 0.996

machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · similarity 0.995

machine-extracted · confidence unavailable · Check page ↗

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