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← Document results/DEP Box 28/GCMS X 1/8/02 A 1/11/02
Document / 18 pages

GCMS results for sample AE00467, Jan 24 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00467 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051453–000051470

Folder label: “GCMS X 1/8/02 A 1/11/02”

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Scanned page image, NYC-WTC_000051465
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN11\00467.D Vial: 7 Acq On : 11 Jan 2002 7:05 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 7 Valine, 3-[sulfothio]- Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 23.68 0.17 ug/L 105722 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Valine, 3-[sulfothio]- 229 C5H11NO5S2 000000-00-0 33 O 2 2-Ally-l-methoxy-3-(methoxymethy... 192 C12H1602 128920-02-5 9 Grv” 3 (IR,3aS,7aS)-7a-Hydroxyethyl -1,4... 224 C14H2402 128790-34-1 9 vao 4 N-Methyl-1,2,4-dithiazolidine-3,... 149 C3H3NO2S2 018137-43-4 7 Abundance Scan 1779 (23.684 min): 00467.D (-) m/z 63.90 100.00% 64

5000 96 149 160

224 W/w 43 84 128 194 23.40 23.60 23.80 24.00

Wz-> 0 " i * • ■ *r " ■ r 11111111 TTT L ' i " " r ■ ■' 40 50 60 70 80 90 100110120130140150160170180190200210220230 ’ ■ i"1' i • ‘" i11" r " ■ r • ■ • i1 Tp-f m/z 159.80 / 75.44% Abundance #157749: Valine, 3-[sulfothio]- 64

75 5000 48 160 23.40 23.60 23.80 24.00 m/ Z 149.00 61.94% 87 96 114 128 194

m/z-> 0 i" ’ ■ r m 40 50 60 70 80 90 100110120130140150160170180190 200210220 230 L22 Abundance #103271:2-Ally-1-methoxy-3-(methoxymethyl)benzene $$ Benz... 160 1B.T 145 23.40 23.60 23.80 24.00 5000 115 129 m/z 223.80 47.04% 91 / 77 192 0 i" "i1" ’ i ’" * i" " i ‘" ■ i • •" r •'11 ■ ′′′ i i" • • i i ■ ■ ■' i" " i1"' i" "r'" i" " i' ■ •n/z-> 40 50 60 70 80 90 100110120130140150160170180190200210220230 Abundance #151530: (1R,3aS,7aS)-7a-Hydroxyethyl-1,4,4-trimethylhexah... 64 192 23.40 23.60 23.80 24.00 m/z 95.90 38.26% 160

/Wisw 128 5000 55 96 81 109 224

o T’TTT p-rrrp-rrrp- i" " i" " i । • ■ ■ ■ । ■1111 "i" Tl/Z-> 40 50 60 70 80 90 100110120130140 150160 170 180190 200210220 230 23.40 23.60 23.80 24.00

00467.D SCAN508.M Mon Jan 14 10:47:07 2002 Page 9

NYC-WTC_000051465

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NYC-WTC_000051465Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · similarity 0.996

machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · similarity 0.995

machine-extracted · confidence unavailable · Check page ↗

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